DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02382.D Vial: 3 ' Acq On : 27 Feb 2002 12:13 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 27, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\HP022102.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N. L Peak Number 6 2-Methoxy-3-hydrazinyl-pyra... Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 13.39 0.0 6 ug/L 33283 Naphthalene-d8 13.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Methoxy-3-hydrazinyl-pyrazine 140 C5H8N40 000000-00-0 50 2 Pyrimidinetetramine- $$ Pyrimidi... 140 C4H8N6 001004-74-6 40 3 2-Fluoronicotinamide 140 C6H5FN20 000364-22-7 40 4 2,5-Cyclohexadiene-l,4-dione, 2,... 140 C6H404 000615-94-1 38 Abundance Scan 887 (13.387 min): 02382.D (-) m/z 140.00 100.00% 140

5000

54 70 78 94 108 13.00 13.20 13.40 13.60 13.80

n/z-> 0- 30 > > i ■ ■ ■ . i ■ 40 50 60 .. | 70I T80,.8^ 90 100 110 120 130 - | 140 ‘.If m/z 70.10 13.73% Abundance #35089: 2-Methoxy-3-hydrazinyI-pyrazine 140

- 5000 42 13.00 13.20 13.40 13.60 13.80 54 68 m/z 94.00 12.34% 80 95 108 121 0| .... | I 1 1 i ■ ' ' i ' ' I,....I..... — +1 "IT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #35040: Pyrimidinetetramine- $$ Pyrimidine, 2,4,5,6-tetraa... 140 i ' ' ' ' i ' ' ■ ■ i 1 ' 13.00 13.20 13.40 13.60 13.80 5000 m/z 65.90 11.86% 44 71 123

miz- > 0b 30I PPPPPP 40 50 60 470 86 96 -------- —l 80 90 112

100 110 120 130 140 TII

Abundance #35138: 2-Fluoronicotinamide 124 140 13.00 13.20 13.40 13.60 13.80 m/z 108.10 11.48% 96 5000 44 51 70 76

mfe-> Ob 30 ■ ■ । ■ 40 i i'I'i 50 —4 . 60 70 1 1 1 1 ■ ' i ■ ' 80 90 100 110 120 I —L TTI 130 140 13.00 13.20 13.40 13.60 13.80

32382.D HP022102.M Thu Feb 28 08:46:48 2002 Page 8

NYC-WTC_000004977