DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\1\5973N\02FEB27\02382.D Vial: 3 Acq On : 27 Feb 2002 12:13 pm Operator: Sample : 508 scan Inst : Instrumen Misc : 2002 February 2 7, Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library- : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 Pyridine, 4-methyl- (CAS) $... Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

9.06 0.07 ug/L 30876 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

l Pyridine, 4-methyl- (CAS) $$ .ga... 93 C6H7N 000108-89-4 90 2 Benzenamine (CAS) $$ Aniline $$ ... 93 C6H7N 000062-53-3 83 3 Aniline 93 C6H7N 000062-53-3 83 4 Pyridine, 4-methyl- (CAS) $$ .ga... 93 C6H7N 000108-89-4 83 Abundance Scan 504 (9.063 min): 02382.D (-) m/z 93.00 100.00% 93

5000 66 1 51 8.80 9.00 9.20 9.40 84 01 ----- i ■ ■ ■ ■ ■ 1■ ■ । ■ ■ ■ ■ । ■ i 11 > ■ ■11 ■ TIT —PPP m/z 66.10 31.52% m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5662: Pyridine, 4-methyl- (CAS) $$ gamma.-Picoline $$ Ba­ sis

5000- ■ ■ i ■ > ■ ■ । ■ 8.80 9.00 9.20 9.40 66 m/z 65.10 19.22%

Tl/z-> 37 46 51 01 TTPPTTT TTi ! n-rt ! 1 , I I , I t , , | , I I I 30 35 62 40 45 50 55 60 65 70 75 80 85 90 95 100 1....... 78...... m -P Abundance #5665: Benzenamine (CAS) $$ Aniline $$ C.1.76000 $$ Anyvi... 93 8.80 9.00 9.20 9.40 5000 m/z 51.00 9.47% 66

38 52 62 0 TIPTTT ■ • j > ■ ■ ■ 111111 ■ । ■ 111111 I ■ ■ i ■ ■ ■ ■ । ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ —PPP m/z—> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #5667: Aniline 93 8.80i 9.00 9.20 9.40 m/z !91.90 8.86%

5000 W 66

37 52 62 0- | | | | | | | ! > Iem i i r i । I I ! I । . ! < i ++ -- - m/z-> 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 8.80 9.00 9.20 9.40

32382.D HP022102.M Thu Feb 28 08:46:48 2002 Page 7

NYC-WTC_000004976