DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File : C : \MSDCHEM\1\5973N\02FEB26\02016 .D Vial: 4 Acq On : 26 Feb 2002 12:49 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 26, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 2,3,4,5,6-D5-ANILINE $$ Ben... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

4.31 0.04 ug/L 22825 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2,3,4,5,6-D5-ANILINE $$ Benzen-d... 98 C6H2D5N 004165-61-1 9 2 2(3H)-Furanone, 5-methyl- 98 C5H602 000591-12-8 7 3 2-Pentenal, 2-methyl- $$ .alpha.... 98 C6H10O 000623-36-9 7 4 2 METHYL 2 PENTENAL 98 C6H10O 000623-36-9 7 Abundance Scan 83 (4.311 min): 02016.D (-) m/z 98.10 100.00% 93

5000

42 ................... ... i । । । > । । । ' । । । । । । i ।

| 49 86 4.00 4.20 4.40 4.60 0111111120108111075310/1214111/1117111 '' i ‘"11" " i"1 ■ i'1" i" ■11" ■ ■ r1" 1111' 11111111" i m/z 100.10 58.93% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #5690:2,3,4,5,6-D5-ANILINE $$ Benzen-d5-amine $$ Aniline-d5 98

5000 —‘ ' i ' ■ ' ' i 1 ■ ■ ■ i 1 ' 1 1 i 1 ' 1 1 I 4.00 4.20 4.40 4.60 71 42 m/z 99.10 17.55% 0 49 66 । 80 ‘ ■ | 1 ' 1 1 | । । 1 | 1 ‘ | ' > 1 I J I । । । [ I 1 ' ‘ TTTTTTTTTTTTTTTT n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #6778: 2(3H)-Furanone, 5-methyl- 93 ■ ■ ' i ■ ■ 1 ■ i ■ ■ ■ 1 i 1 ' 1 1 i ' 1 1 1 i 43 4.00 4.20 4.40 4.60 55 5000 m/z 42.00 16.87% 27

Of 15 mmejilip 38 —49+ ........ 70......82.......... miz- > 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 +mmpm Abundance #6953:2-Pentenal, 2-methyl- $$ .alpha.-Methyl-.beta.-ethy... 1 ■ । ■ 1 1 ' । 41 4.00 4.20 4.40 4.60 98 m/z 43.20 15.78%

.5000 69

27 55 83

/z-> 01 ' " I' ' " I " " I ' ‘ " I ' Im—?+ - TTTTT1 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 4.00 4.20 4.40 4.60

02016.D HP022102.M Wed Feb 27 08:34:32 2002 Page 6

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