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← Document results/DEP Box 28/GCMS X 1/4/02 A 1/25/02
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GCMS analysis results for sample AE00105, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.

NYC-WTC_000050793–000050812

Folder label: “GCMS X 1/4/02 A 1/25/02”

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Scanned page image, NYC-WTC_000050800
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN25\00105.D Vial: 3 • Acq On : 25 Jan 2002 11:49 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 n-Valeric Anhydride Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

4.25 0.10 ug/L 41744 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 n-Valeric Anhydride 186 C10H18O3 000000-00-0 10 2 2-Propenoic acid, 2-methyl- (CAS... 86 C4H602 000079-41-4 9 3 1-Butanamine, 3-methyl- (CAS) $$... 87 C5H13N 000107-85-7 9 4 Methacrylamide 85 C4H7NO 000079-39-0 9 Abundance Scan 77 (4.253 min): 00105.D (-) m/ z 85.00 100.00% 41 85

5000 55 60 89 ...................... . 4.00 4.20 4.40 4.60 51 " i■''■r " ■i■' " i ■■ ■■ 11 ■ ■ ■ i'1 TTT ‘‘‘‘I m/z 41.10 99.53% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #95372: n-Valeric Anhydride 85

5000 29

41 57 „AA..M,,AN. 4.00 4.20 4.40 4.60 m/z 43.10 60.80% 60 15 26 —4 +4 73

_AMA >11 >1 >11" > > । । n' I "i■ ............... I lire.... -I n/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3758:2-Propenoic acid, 2-methyl- (CAS) $$ Methacrylic ac... 41 85 4.00 4.20 4.40 4.60 5000 m/z 87.10 51.70%

m/z-> " i' ■" i" " r "11" " r " ■ r1' 3£ 58 ...... I"1'! + 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 45

#4416:1-Butanamine 3-methyl- (CAS) $$ Isoamylamine $$ Le... —TP a 69

41 4.00 4.20 4.40 4.60 44 m/z 39.10 32.44%

5000 70 55 87 58

m/z-> 5 । ■ ■ ■ ■ ।। । • ■ ■ ■ । J 38

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 "11" A " i" ■ ■ i" ■ • i ■ • ■ > i 4.00 4 20 i ■ ■ ■ ■ i ' ■ 4 40 4.60

00105.D SCAN508.M Mon Jan 28 09:49:47 2002 Page 4

NYC-WTC_000050800

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NYC-WTC_000050800Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

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