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GCMS analysis results for sample AE00105, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.

NYC-WTC_000050793–000050812

Folder label: “GCMS X 1/4/02 A 1/25/02”

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NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN25\00105.D Vial: 3 Acq On : 25 Jan 2002 11:49 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 Butanoic acid, methyl ester Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 3.61 0.13 ug/L 54085 1,4-Dichlorobenzene-d4 9.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Butanoic acid, methyl ester 102 C5H10O2 000623-42-7 83 2 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 3 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 4 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 Abundance Scan 21 (3.614 min): 00105. D (-) m/z 43.10 100.00% 43 74

5000 59 87 i' ■ ■ ■ i

3.50 3.60 3.70 3.80 3.90 4.00 A.... 4 Wz-> 10 20 30 — 40 -4-- 50 60 70 80 90 100 110 m/z 74.10 95.56% Abundance #9219: Butanoic acid, methyl ester 43 74 5000 27 TT r ■' ■ i " " i " " r ■ " r ■ ■ ■ i 15 3.50 3 60 3.70 3.80 3.90 4.00 59 87 m/z 71.10 66.95% 33 38 | | 102 i 1 1 1 1 I 1 1 1 1 I 1 1 1 1 I । n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9222: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74 T T I i1' " i " " r " • i' " ' i 3.50 3.60 3.70 3.80 3 90 4.00 5000 m/z 41.10 31.60% 59 87

33 + 102 ' ■ i ■ ' ■ ■ i 1 I ■ ' 1 ■ i 1 i ' ■ ■ ■ i 1 1 1 1 i 1 < I • ■ • t । • 1 । 1 -' 1 1 I n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance ;#9227: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... ।11 ■ ■ ।1 ‘ । r"•i 43 74 3.50 360 3.70 3.80 3.90 4.00 m/z 87.10 28.63%

5000 59 87 - 69 102 ।11 1 i 1 1 IT 1 -nr11 ■ ■ i ■ ■ ■ 1 i ■ ■ ■ 1 । ■ 1 ■ ■ i i' " ' i'1'' i " " i r 1" i mlz-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90 4.00

0105.D SCAN508.M Mon Jan 28'09:49:47 2002 Page 3

NYC-WTC_000050799

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NYC-WTC_000050799Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

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