Laboratory report listing unknown compounds and surrogate recovery for sample AE00105 analyzed on February 7, 2002.
NYC-WTC_000050793–000050812Folder label: “GCMS X 1/4/02 A 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN25\00105.D Vial: 3 Acq On : 25 Jan 2002 11:49 am Operator: Sample : 508 scan Inst : Instrumen Mise : January 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 1 Butanoic acid, methyl ester Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 3.61 0.13 ug/L 54085 1,4-Dichlorobenzene-d4 9.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Butanoic acid, methyl ester 102 C5H10O2 000623-42-7 83 2 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 3 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 83 4 Butanoic acid, methyl ester (CAS... 102 C5H10O2 000623-42-7 78 Abundance Scan 21 (3.614 min): 00105. D (-) m/z 43.10 100.00% 43 74
5000 59 87 i' ■ ■ ■ i
3.50 3.60 3.70 3.80 3.90 4.00 A.... 4 Wz-> 10 20 30 — 40 -4-- 50 60 70 80 90 100 110 m/z 74.10 95.56% Abundance #9219: Butanoic acid, methyl ester 43 74 5000 27 TT r ■' ■ i " " i " " r ■ " r ■ ■ ■ i 15 3.50 3 60 3.70 3.80 3.90 4.00 59 87 m/z 71.10 66.95% 33 38 | | 102 i 1 1 1 1 I 1 1 1 1 I 1 1 1 1 I । n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #9222: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... 43 74 T T I i1' " i " " r " • i' " ' i 3.50 3.60 3.70 3.80 3 90 4.00 5000 m/z 41.10 31.60% 59 87
33 + 102 ' ■ i ■ ' ■ ■ i 1 I ■ ' 1 ■ i 1 i ' ■ ■ ■ i 1 1 1 1 i 1 < I • ■ • t । • 1 । 1 -' 1 1 I n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance ;#9227: Butanoic acid, methyl ester (CAS) $$ Methyl butyrat... ।11 ■ ■ ।1 ‘ । r"•i 43 74 3.50 360 3.70 3.80 3.90 4.00 m/z 87.10 28.63%
5000 59 87 - 69 102 ।11 1 i 1 1 IT 1 -nr11 ■ ■ i ■ ■ ■ 1 i ■ ■ ■ 1 । ■ 1 ■ ■ i i' " ' i'1'' i " " i r 1" i mlz-> 10 20 30 40 50 60 70 80 90 100 110 3.50 3.60 3.70 3.80 3.90 4.00
0105.D SCAN508.M Mon Jan 28'09:49:47 2002 Page 3
NYC-WTC_000050799
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NYC-WTC_000051364
Laboratory report showing GCMS analysis of sample AE00314 with surrogate recovery data on January 24, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051236
Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE00366 conducted on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051642
Laboratory report showing GCMS analysis results for sample AE00616 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051567
Laboratory report showing GCMS analysis results for sample AE00562 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051422
Laboratory report showing GCMS analysis of sample AE00463 with surrogate recovery data on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051055
Laboratory report showing GCMS analysis of sample AE00307 for unknown compounds and DDD on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051301
Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050664
Laboratory report listing unknown compounds and surrogate recovery for sample AE00165 analyzed on February 13, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037720
Laboratory report documenting GCMS analysis of a method blank for sample AE03612 to verify analytical system cleanliness.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000010967
Gas chromatography-mass spectrometry analysis of sample AE02718 performed March 5, 2002, documenting other unknown compounds and surrogate 2,4-DDD recovery at 97 percent.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037780
Gas chromatography-mass spectrometry analysis of sample AE03616 performed on 3/28/2002, detecting other unknown compounds with surrogate 2,4-DDD at 5.0 µg detection limit.
1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000004494
Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
1 shared non-person entities · 1 shared topics · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000050702
Administrative record from DEP Box 28 documenting CCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050703
Technical log recording method parameters and sample processing details for a DEP laboratory procedure between January 4 and 25, 2002.
Filed in the same folder
NYC-WTC_000050705
Laboratory report listing concentrations of volatile organic compounds in sample AE00027 analyzed on January 25, 2002.
Filed in the same folder
NYC-WTC_000050709
Reference standard GCMS analysis for sample AE00027 performed on January 25, 2002, providing quality control results.
Filed in the same folder
NYC-WTC_000050716
Laboratory report showing non-detect results for volatile organic compounds in a GCMS blank analyzed on January 25-February 7, 2002.
Filed in the same folder