GCMS DFTPP calibration report, Feb 5 2002

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Chromatogram and method report for DFTPP calibration verification conducted on February 5, 2002.

NYC-WTC_000004770–000004933

Folder label: “GCMS X 2/1/02 A 2/5/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\0201B.D Vial: 1 Acq On : 5 Feb 2002 10:42 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\HP020702 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 6 Dimethyl phthalate Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 17.88 0.08 ug/L 82225 Acenaphthene-dl0 18.34 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dimethyl phthalate 194 C10H10O4 000131-11-3 72 2 Dimethyl phthalate 194 C10H10O4 000131-11-3 72 3 1,2-Benzenedicarboxylic acid, di... 194 C10H10O4 000131-11-3 72 4 Dimethyl phthalate $$ 1,2-Benzen... 194 C10H10O4 000131-11-3 72 Abundance Scan 1271 (17.885 min): 0201 B.D (-) m/z 163.10 100.00% 163

5000 152 77 —————— 50 92 133 , 194 17.60 17.80 18.00 18.20 0! -- vjuill, lm I........... I " '111 H ' 111 ■' I'1 ■ •|■I■•l■'"|1• >1|ih'।" m/z 152.10 34.19% n/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #105351: Dimethyl phthalate 163

5000 ....... ,.......... 17.60 17.80 18.00 18.20 77 m/z 77.00 23.70% 50 92 104 120 135 . 194 01 MH ''1641111111|1111 ‘" TJ111 THTT —Ppr iz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #105362: Dimethyl phthalate 1(3 A 17.60 17.80 18.00 18.20 5000 m/z 164.10 10.38% 77 9- . 0 135 194 50 66 1 ।. 11.,, ।, I1,11111117i 111 mmprri ■ । ■ ■ ■. । ■ Of ■ ■ | ■ 1 ■ • | ■ 1 1 l‘| > 1 1 1 | • 1 Hl | 1 104 120 ,| " I' " ' i' ‘ " i'1 " i " /z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #105358:1,2-Benzenedicarboxylic acid, dimethyl ester (CAS... 163 17.60 17.80 18.00 18.20 m/z92.00 9.62% 5000

m/z-> 50 J 92 104 120 135 149 0 ■ ■ i ■ " ' I' " ‘ i' IIs*ssta’sssuo*ssodougsasoloeum "1 • ।111 > ।' > ■ ■ । ■ 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 194 — 111" I' m । l'i 1111 . ... M 17.60 17.80 18.00 18.20

0201B.D SCAN508.M Thu Feb 21 10:18:58 2002 Page 8

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