GCMS DFTPP calibration report, Feb 5 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\l\5973N\02FEB05\0201B.D Vial: 1 Acq On : 5 Feb 2002 10:42 am Operator: Sample : lab blank 2/1 Inst : Instrumen Mise : February 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP020702.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 0-CHLOROPHENOL-D4 $$ 3,4,5,... Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 9.24 0.12 ug/L 76315 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 0-CHLOROPHENOL-D4 $$ 3,4,5,6-Tet... 132 C6HD4C1O 000000-00-0 46 2 0-CHLOROPHENOL-D4 $$ 3,4,5,6-Tet... 132 C6HD4C1O 000000-00-0 43 3 0-CHLOROPHENOL-D4 $$ 3,4,5,6-Tet... 132 C6HD4C1O 000000-00-0 43 4 Ethane, 1,1'-[methylenebis(oxy)]... 172 C5H10C12O2 000111-91-1 35 Abundance Scan 514 (9.242 min): 0201 B.D (-) m/z 132.00 100.00% 132

93 5000 63 68

40 8.80 9.00 9.20 9.40 9.60

m/z-> Oh 30। —401.49 50 60 ■ ■ i ■ ■ 70 80 Il ll..... fyii............... 90 100 110 120 130 140 m/z 93.10 53.40%

Abundance #24011: O-CHLOROPHENOL-D4 $$ 3,4,5,6-Tetradeuterio-2-chlor... 132

5000 68 .......,.,1...... 8.80 9.00 9.20 9.40 9.60 93 m/z 63.10 41.01% 104

n/z-> Oh 30 48 I 76 " I 1 1 11 I 1 1 1 1 — I I । । । I । । । । । । । । 40 50 60 70 80 90 H 100 110 120 130 140 I

Abundance #24012: O-CHLOROPHENOL-D4 $$ 3,4,5,6-Tetradeuterio-2-chlor... 132 I 1 1 1 1 f 8.80 9.00 9.20 9.40 9.60 5000 m/ z 68.10 39.14% 68

96

miz-> oh 30 11 40 48 50 60 —— 70 80 90 100 104 ' I ‘ 110 120 L — ________________ ‘ I 1 1 ' ' I 130 L 1 1 I 1 1 140 ... ...... . Abundance #24013: O-CHLOROPHENOL-D4 $$ 3,4,5,6-Tetradeuterio-2-chlor... 132 8.80 9.00 9.20 9.40 9.60 m/z 134.00 35.10% 68 5000

96 75 104

n/z-> oh 30 —l 40 50 60 — 70 80 90 H—........ 1 100 110 120 130 140 8.80 9.00 9.20 9.40 9.60

0201B.D SCAN508.M Thu Feb 21 10:18:57 2002 Page 7

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