GCMS sample AE12765 results, June 6 2002

NYC 9/11 Public Portal Document Library search compound Report

Data File C:\MSDCHEM\1\DATA\060402\12765.D Vial: 6 Acq On 4 Jun 2002 7:55 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 10 Ether, chloromethyl dichlor... Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T. 5.02 0.33 ug/L 212966 1,4-dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ether, chloromethyl dichloromethyl 148 C2H3C130 002799-32-8 2 Propiolonitrile 51 C3HN 001070-71-9 5 3 2,3-Dichloropropionitrile 123 C3H3C12N 002601-8 0 4 4 4,5-Dichloro-l,3-dioxolan-2-one 156 C3H2C1203 003967-% -3 4 Abundance Scan 330 (5.018 min): 12765.D (-325) (-) m/ z 49.10 100.00% 49 82 127 5000

miz-> Abundance —4 0 ■ ■ ।' i1' ■11 ■ ■ ■ r 1 ■ ■ i ‘ ‘ " i 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 i ■ ■' • i ■ ■ ■' i ■''' i ■ ■ ’ I >* 1111

#12328: Ether, chloromethyl dichloromethyl । >. ■ > । vulGLI 4.60 4.80 5.00 5.20 5.40

49 85 113 5000 4.60 4.80 5.00 5.20 5.40 m/z 126.90 67.81% 63 77 o1 -jon.... is... 'I TTpt4 +p121——— 147 “ i “ ‘‘i • " ■ i miz-> 0 10 20 30 40 I50 60 70 80 90 100 110 120 130 140 150 Abundance #12371: PropioIonitrite 51 I 1 1 11 I 111 1 1' 1 1 1 1 1 1 4.60 4.80 5.00 5.20 5.40 5000 m/z 82.00 63.75%

25 38 W

n/z-> 0- - 0 12 + 1 ■ ■ ■ ।1 ■1' i ■ ■ ■ ■ i" " ।" ■ ■ i ■"1 r“111"111111111111111111 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 Abundance #12329:2,3-Dichloropropionitrile f1 ' ' 11 43 88 4.60 4.80 5.00 5.20 5.40 m/z 128.90 61.88%

5000

26 62 35 n 0 4 14 +4 -H 74 97 123 “ i ■ ■ ■ ■ i ■ ■ “ i “' ■ i “ “ i ■ “ ' i ■' " i /z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 4.60 4.80 5.00 5.20 5.40

12765.D 060302.M Wed Jun 05 14:05:37 2002 Page 13

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