GCMS sample AE12765 results, June 6 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\MSDCHEM\1\DATA\060402\12765.D Vial: 6 Acq On 4 Jun 2002 7:55 pm Operator: McLean Sample 6/4 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 11 Krypton Concentration Rank 9 R.T. EstCone Area Relative to ISTD R.T.

5.05 0.55 ug/L 356984 1,4-dichlorobenzene-d4 9.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Krypton 84 Kr 007439-90-9 7 2 Perdeuterobenzene 84 C6D6 001076-43-3 4 3 l-Penten-3-one 84 C5H80 001629-58-9 4 4 Piperidine 85 C5H11N 000110-89-4 4 Abundance Scan 336 (5.054 min): 12765.D (-334) (-) m/z 84.00 4100.00% 84

49 5000 37 41 .. 44 4.80 5.00 5.20 5.40 ........................................ 35 , | ol ’ I’’’’I’’IUUII’/U79SSSS9761973 mmm ■ ■i ■ " ■ i■ m/z 49.10 54.57% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33829: Krypton 84

5000 4.80 5.00 5.20 5.40 42 ^m/z^^ 80 0 mTTTTTTTTTT ‘ i ‘1 • ■ i ■ ■ “ i ■ ■ ■11 • ■ ■ ■ i ■ ■' ■ i “1' I ■ “*।■***।> iz—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #33650: Perdeuterobenzene 84

4.80 5.00 5.20 5.40 5000 m/z 86.90 35.43% 52 56 42

ol ...... 12 18 24 28 38, 48 62 66 72 76 80 <■ |>11 ' । . I t i । i ■ l .।.Il!|I'+11' ' ' ' J I 1 I ! J 1 1 I 1 | I I 1 I | I I ' I | tuvgatalpamr Imm niz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63:1-Penten-3-one - 27 4.80 5.00 5.20 5.40 55 m/z 47.10 34.43% 5000

84 0 ■ ■ । ■ ■1'i■■■1111" i111'I 30 3942 52 - ] 11 i i | 1 I I I 11 I I | | । । rr[ l I 11 11' M I" " 11 n/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 4.80 5.00 5.20 5.40

12765.D 060302.M Wed Jun 05 14:05:38 2002 Page 14

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