GCMS analysis results for sample AE06335, April 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\DATA\020408\6335.D Vial : 19 Acq On 9 Apr 2002 3:37 am Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1...\SCANAPR0902 .M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 Peak Number 1 Krypton Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.29 0.14 ug/1 174857 1,4-Dichlorobenzene-d4 10.66 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Krypton 84 Kr 007439-90-9 5 2 Chloromethyl ethanoate 108 C3H5C102 1000143-34-6 2 3 Acetic acid, chloro-, ethyl ester 122 C4H7C1O2 000105-39-5 1 4 Boron trifluoride etherate 142 C4H10BF3O 000109-63-7 1

nMMolmnoy Abundance Scan 36 (3,291 min): 6335. D (-21) (-) m/z 84.00 100.00% 43 49 84 74 5000

1 1'I111111111111'111111 ’111 3.20 3.30 3.40 3.50 3.60 3.70 0 ' ' i ' ' ' ' i 1 1 1 ' i ' 1 ' ' ' ■ l' 1 1 ' l ' ' 1 ' l ‘ 1' i 1 ■ i ■ ■ ■ ■ । 1 ■ > > । ■ i 1 ■ ■ ■ । 1 m/z 49.00 84.35% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 / Abundance #33829: Krypton 84

5000 3.20 3.30 3.40 3.50 3.60 3.70 42 m/ z 43.10 76.79% 78, O+ ■ ' i 1 ■ ' ' 1 1 1 1 1 1 1 1 1 1 1 1 ■ । 11 ■ 1 i1'111'1111 11’11■।■ 1 1 । ■ 1 1T 11 111 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120130 Abundance #4957: Chloromethyl ethanoate 43

3.20 3.30 3.40 3.50 3.60 3.70 5000 m/z 74.10 61.14% 49 73 —— | I I I ! | । 65 | Of ■ ‘ r''11 । * ■' * । >' > > । < *' ' ।1''11 ' 1 1 11 ’ ।1111 11 ।1 m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #108005: Acetic acid, chloro-, ethyl ester 23 3.20 3.30 3.40 3.50 3.60 3.70 m/z 71.10 55.59% 5000 77 42 49 14

m/z-> 0 — 10 20 +30435—40 4+4. 50 59 65 TT’T i । । । । । 60 70 | 88 94 107 122 'iij■•■■ j ■<' > 1l > 1i' । ■ I। i TI । iii]i 80 90 100 110 120 130 3.20 3.30 3.40 3.50 3.60 3.70

6335.D SCANAPR0902 .M Tue Apr 09 15:21:15 2002 Page 3

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