GCMS Method 508 sample analysis results, April 9 2002

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• Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\020409\6340.D Vial: 9 Acq On 9 Apr 2002. 10:37 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1...\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Krypton Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 3.30 0.23 ug/1 159702 1,4-Dichlorobenzene-d4 10.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Krypton 84 Kr 007439-90-9 5 2 2-Butyne-l,4-diol 86 C4H6O2 000110-65-6 3 3 Propanal, 2,2-dimethyl-, oxime 101 C5H11NO 000637-91-2 2 4 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 2 Abundance Scan 37 (3.297 min); 6340. D (-20) (-) m/z 49.00 100.00% 84 8000 43

6000 74

4000 I *''' I'''' I'''' r I'''' I 3.20 3.30 3.40 3.50 3.60 3.70 m/z 84.00 86.24% n/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #33829; Krypton 84

5000 3.20 3 30 3.40 3.50 3.60 3.70 42 in/z 43.10 73.62%

■nfe-> .. . ... ill,,,,,,,,.,,,,,,, 15 20 25 30 35 40 . . 111,1,,,,.... . .. . 55 60 65 70 75 60 85 '90''9'5''l'66 105 '' Abundance #108388: 2-Butyne-1,4-diol 29’ 3J 5|7

3.20 3.30 3.40 3.50 3.60 3.70 5000 Wz 74.10 52791% 68 51

TlZZ-> JU 73 15 20 25 30 35 40 45 50 55 60^^ 70 75 80 85 90 95 100 105 85

Abundance #1431: Propanal, 2,2-dimethyl-, oxime 40 3.20 3.30 3.40 3.50 3.60 3.70 84 m/z 47.00 50.84%

5000 26

JU 72 56 67

mfe-> 45 50 At AX 15 20 25 30 35 40 45 50 . 55 60 65 70 75 80 85 90 95 100 105 J 3.20 3.30 3.40 3.50 3.60 3.70

6340.D SCANAPR0902.M Thu May 02 14:08:41 2002 Page 3

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