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← Document results/DEP Box 14/GCMS X 2/5/02 A 2/28/02
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GCMS analysis results for sample AE03075, March 5 2002

Machine-extracted title · confidence 50%

Laboratory report documenting gas chromatography-mass spectrometry results for sample AE03075 including surrogate recovery.

NYC-WTC_000010927–000010946

Folder label: “GCMS X 2/5/02 A 2/28/02”

←Page 16 of 20→
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\5973N\02FEB28\02716 .D Vial: 1 Acq On : 28 Feb 2002 2:40 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 2 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 10 4-METHOXY-.BETA.-METHYLCINN... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

22.28 0.12 ug/L 75603 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 4-METHOXY-.BETA.-METHYLCINNAMIC ... 192 C11H12O3 019169-94-9 64 2 3-Cyanocarbazole $$ 9H-Carbazole... 192 C13H8N2 057102-93-9 59 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 59 4 2-CYANOCARBAZOLE $$ 9H-Carbazole... 192 C13H8N2 057955-18-7 45 Abundance Scan 1675 (22.283 min): 02716.D (-) m/z 192.00 100.00% 19/2

5000

44 01TIIun—n—BT - 82 96 ----- 118 I । I i I i । i 146 160 i I'l । i > ■ i | ! I . . । . . . . । . . A A m/z 96.00 17.26% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102588:4-METHOXY-.BETA.-METHYLC1NNAM1C ACID $3 2-Butenoi... 192

108 5000 22.00 22.20 22.40 22.60 146 175 m/z 191.00 16.88%

miz-> 4 0- ■ ■ i1 ■ " i•■■■i"■ ■ i " i ■ " ‘ i ■•1■i■' i ■ ■ ■ ■ i ■ ■ “ i ■ • " i ■ ‘ ' i “ “ i1' ■' r 11. ।i1 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192

22.00 22.20 22.40 22.60 5000 m/z 193.00 16.42%

96 164 I 138 01 —PTPmmT wuunt ’IT miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 22.00 22.20 22.40 22.60 m/z 146.10 14.24%

5000

n/z-> 0 TI—nmmmmuatnOuumaanupnadm 882 139 152 165 176 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 t -A 22.00 22.20 22.40 22.60

02716.D HP022102.M Fri Mar 01 10:07:15 2002 Page 12

NYC-WTC_000010942

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NYC-WTC_000010942Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.998

machine-extracted · confidence unavailable · Check page ↗

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