GCMS analysis results for sample AE03252, March 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03252 conducted on March 15, 2002.

NYC-WTC_000006226–000006245

Folder label: “GCMS X 2/12/02 A 3/01/02”

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NYC 9/11 Public Portal Document ulDLary cearcn compound Report Data File : C:\MSDCHEM\1\5973N\02MAR01\03252 .D Vial: 7 • Acq On : 1 Mar 2002 8:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : March 1, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 8 N-perdeuteriobenzylideneani... Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 22.28 0.13 ug/L 101994 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 2 N-(2-methylprop-2-enyl)-2-nitrob... 192 C10H12N2O2 000000-00-0 49 3 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 000000-00-0 45 4 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-9 42 Abundance Scan 1675 (22.283 min): 03252. D (-) m/z 192.00 100.00% 192

5000

82 96 146 160 0- 49 —— 70 | -+1ls I— n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 । n-i i । i i’l" | n । I T> ! i i । । i , i ।, 22.00 22.20 22.40 22.60 m/z 191.00 21.76% Abundance #88409: N-perdeuteriobenzylideneaniline 192

5000 82 22.00 22.20 22.40 22.60 54 110 m/Z95.90 14.71%

n/z—> 30 0 — " r 1 " i1 ■ I ■ | lI I ■ | 94 I I I I | I I !

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 160 " ।1"11"1' ।"111"111'11" i"111"1,1 U Abundance #102494: N-(2-methylprop-2-enyl)-2-nitrobenzenamine 192 77 151 130 22.00 22.20 22.40 22.60 93 104 m/z 193.10 13.89% 5000 119

177 0 11J‘‘‘‘I‘‘‘‘I‘‘‘IIIII‘ "1111' i Tp-r TTTr ■ i"'11" " r " 11" " i 11 ‘1’1 I..... m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #102788: 2,5-Dihydrophosphole, 3-methyl-1-oxo-1-phenyl- 192 22.00 22.20 22.40 22.60 164 m/z 146.00 13.65%

5000 99 115 47 77 177

0 I | ................... IIII TTTTTTTT]m)WTPITTITTTTTTTT I" r " 11" " I 125134 146, A ) n/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.00 22.20 22.40 22.60

3252.D HP022102.M Mon Mar 04 12:33:55 2002 Page 10

NYC-WTC_000006239

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NYC-WTC_000006239Source: NYC Law Department, mirrored locally

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GCMS analysis results for sample AE03248, March 2002 · Box DEP Box 12

NYC-WTC_000006146

Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE03248 conducted on March 15, 2002.

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