GCMS analysis results for sample AE09333, May 2002

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Data File C:\MSDCHEM\1\DATA\050202\9333.D Vial: 11 Acq On 2 May 2002 7:48 pm Operator: Mclean Sample 4/29 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 16 9-Octadecenamide, (Z)- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

33.68 0.26 ug/L 221498 Perylene-dl2 34.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 9-Octadecenamide, (Z) - 281 C18H35NO 000301-02-0 56 2 7-Nonenamide 155 C9H17NO 090949-53-4 5 3 Dodecanamide 199 C12H25NO 001120-16-7 40 4 Mannosamine hydrochloride 179 C6H13NO5 1000127-68-8 25 Abundance Scan 5209 (33.685 min): 9333.D (-5202) (-) m/z 59.10 100.00% 59 72

5000 43

97 1 1 1 1 112 126 207 33.40 33.60 33.80 34.00 3 , Il , I ..... ..... ..... ..... 1............. ....... m/z 72.10 77.72% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #109752: 9-Octadecenamide, (Z)- 43 59

5000 72 ............ H.............. । I I I I-] r । । i । i । I I | I I

29 33.40 33.60 33.80 34.00 I1' m/ z 55.10 62.78% 1|6 1 ll X._ h ■ 1, A ; 1 22136150 164178 1 93207 221236....... 281 TiMqiiiT| riTT|TTT1 | । r i r । _r i t । । । । II | il i i | ‘ ri i | । ‘ 1 < । r । pi

m/z-> 20 40 60) 80 100 120 140 160 180 200 220 240 260 280 Abundance #19655: 7-Nonenamide 59

33.40 33.60 33.80 34.00 5000 72 m/z 43.10 44.28% 44

m/z->20 Abundance 29 । । । 1 | II. ' fl_ । n 40 i 1.1 I 85 98 112 126 140 155 60 ——————————

80 100 120 140 160 #19649: Dodecanamide r I i I I I I I I I I I l l” l”l' I I I

180 200 220 240 260 280 7 59 33.40 33.60 33.80 34.00 m/ z 41.10 36.46% 5000 72 28 43

15 86 100 114 128 142 156 170 199 ■ ■ i ’

/z-> 20 80 100 120 140 160 180 200 220 240 260 280 33.40 33.60 33.80 34.00

9333.D 050102.M Mon May 06 13:56:02 2002 Page 2 0

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