NYC 9/11 Public Portal Document
LlDrary searen compound Keporc
Data File : C:\MSDCHEM\l\DATA\051702\0515LB.D Vial: 16
Acq On : 18 May 2002 1:49 am Operator: Mclean
Sample : 5/15 eh Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library- : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 6 Octasiloxane, 1,1,3,3,5,5,7.. Concentration Rank 7
R.T. EstConc Area Relative to ISTD R.T.
33.11 0.57 ug/L 389729 Perylene-d12 34.70
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Octasiloxane, 1,1,3,3,5,5,7,7,9,... 578 C16H50O7Si8 019095-24-0 10
2 Heptasiloxane, 1,1,3,3,5,5,7,7,9... 504 C14H4406Si7 019095-23-9/10
3 Methanimidamide, N,N-dimethyl-N'... 148 C9H12N2 001783-251 9
4 Guaifenesin di-tms derivative 342 C16H30O4S12 1000137- 06-7 9
Abundance Scan 5110 (33.103 min): 0515LB.D (-5109) (-) m/z 221.10 1 00.00%
221
148
5000 73 355
297
40 429 32.80 33.00 33.20 33.40
ol., , I । . J ■ . ... 1..267, Ili” m/z 207.00 74.81%
m/z-> 50 100 150 200 250 300 350 400 450 500 550 /
Abundance #27373: Octasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13,15,1...
73
5000 207 1 ' I ' 1 1 1 1 1 1 1 1 [ ' 1 1 ' 1 1 1 1 1 I
32.80 33.00 33.20 33.40
281 m/z 148.05 54.48%
147
341 2
45. 117|| 177,
0K ’ 1 I ' ‘ ■ 1 i 1' ' ■ i 1 ■ ■ ' । 4 2514— 313, .371 401429 503 563
m/z-> 50 100 150 200 250 300 350 . 400 450 500 550
Abundance #27374: Heptasiloxane, 1,1,3,3,5,5,7,7,9,9,11,11,13,13-tet...
73
TII 1 ■ i ■ ' 1 1 i
32.80 33.00 33.20 33.40
5000 207 m/z 147.10 50.19%
133 281 355
ol 45, .103.1,4,177
' 111 1
, 1.2531 .. | 327),k 383 , 429 489 ...
mfe-> 50 100 150 200 250 300 350 400 450 500 550
Abundance #110608: Methanimidamide, N,N-dimethyl-N'-phenyl-
44 n 148 32.80 33.00 33.20 33.40
A.
m/z 73.10 44.78%
5000 106
mfe->
Ok- ' r । ' 11
50
—4+
100 150 200 250 300 350 400 450 500 550
__________ N_________________ VAAA AA
1 ' ' I 1 ‘ ‘ I I ‘ ‘ I I ms-T" Ti I . f
32.80 33.00 33.20 33.40
AA
0515LB.D 050102.M Tue May 21 16:00:13 2002 Page 9
NYC-WTC_000025228
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