NYC 9/11 Public Portal Document
Llorary searcn compound Keport
Data File : C:\MSDCHEM\1\DATA\051402\10981.D Vial: 10
Acq On : 14 May 2002 8:50 pm Operator: Mclean
Sample : 5/10 kb Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: LSCINT.e
Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator)
Title : 508 Modified GC/MS scan
Library : C:\DATABASE\NIST98.L
*********************************************************************
Peak Number 9 3,6-Dioxa-2,4,5,7-tetrasila... Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
35.42 0.70 ug/L 564443 Perylene-dl2 34.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 3,6-Dioxa-2,4,5,7-tetrasilaoctan... 294 C10H3002Si4 004342-25-0 43
2 1,1,1,5,7,7,7-Heptamethy1-3,3-bi. . . 444 C13H40O5Si6 038147-00-1 40
3 Mercaptoacetic acid, bis(trimeth... 236 C8H20O2SSi2 006398-62-5 32
4 Pentasiloxane, dodecamethyl- 384 C12H3604Si5 000141-63-9 27
Abundance Scan 5504 (35.419 min): 10981.D (-5494) (-) m/z 73.10 100.00%
73 147 221
5000
281 355
429 LMAAMMYMTY
44 193 35.00 35.20 35.40 35.60 35.80
96 119
0— m/z 147.10 82.72%
n/z-> 0 50 100 150 200 250 300 350 400
Abundance #87890: 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 2,2,4,4,5,5.7,7...
147 22!1
5000
73
_ m
35.00 35.20 35.40 35.60 35.80
191 m/z 221.10 79.35%
117
mfe->
oS
0
45
T’)
50
A
100 150
' 1 11
200
1 1
250 _ 300
279
249., .000001
350 400
Abundance #26950:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)...
73
' ......................... ......... ...
147 35.00 35.20 35.40 35.60 35.80
5000 267 m/z 207.00 40.28%
355 429
45 207
............................................. ........... I ! I, , . , , ,
Aowopow/orwoanoe--
oS- ' i ■
miz—> 0 50 100 150 200 250 300 350 400
Abundance #26922: Mercaptoacetic acid, bis(trimethylsilyl)- ' 1 i ■ 1 ' ' i ' ■
73 35.00 35.20 35.40 35.60 35.80
147
m/z 281.00 38.23%
A
5000
221
45
0— 13—144 -
104 __ 193
1169 1)...... .......... now wW/un
m/z-> 0 50 100 150 200 250 300 350 400 35.00 35.20 35.40 35.60 35.80
10981.D 050102 .M Thu May 16 14:37:21 2002 Page 12
NYC-WTC_000023986
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