GCMS analysis results, sample AE09972, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\MSDCHEM\l\DATA\050602\9972.D Vial : 20 Acq On 7 May 2002 3:11 am Operator: Mclean Sample 4/25 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 13 Anthracene-dlO- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.59 ug/L 683678 Phenanthranene-dl0 22.96

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 90 2 Phenanthrene-dlO 188 C14D10 001517-22-2 80 3 Pyrrolo[2,3-b]indole, 1,2,3,3a,8... 188 C12H16N2 004089-16-1 58 4 Cycloheptanone , 4-phenyl-188 C13H160 067688-28-2 47 Abundance Scan 3409 (23.109 min): 9972.D (-3402) (-) m/z 188.10 100.00% 188

5000

80 94 1 i ' 1 ‘ 1 i 1 1 43 57 66 22.80 23.00 23.20 23.40 132 146 16° rF । i > i i । i i i i 111 i r I " । i I I r r+ r । । । r । ~i । । t । ~r । I । । i । । i ! । । । । I I । i t । 81 । ■ 1 r | 1 111111 m/ z 94.10 17.81% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d 10- 188

5000 ------- 22.80 23.00 23.20 23.40 m/z 184.10 17.41% 80 94 160 , । 66 17 30 42 52 ' I " " I " " I " " I" " 111" | rl l | | । > I I | I । । I | 108 118 132 I I | I I I I | I I 1 I | I T I ^l^|^l^l~t^1^| 146444.17917944 rm m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 I । | I I I I - I I —I ! | I I I I | I I I I r

22.80 23.00 23.20 23.40 5000 m/z 189.15 16.64%

80 94 160 30 42 52 66 , ll 108 118 132 / । i > i i । 1 । i i । i m i | t । > । । rl ! । । I I I । pi I rI I । '111 "I" "I"" I ""I'1" 146,,+1.,170179ll m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79762: Pyrrolo[2,3-b]indole, 1,2,3,3a,8,8a-hexahydro-3a,8... ---------------------------- 144 188 22.80 23.00 23.20 23.40 m/z 80.05 15.11% 158 5000

130 42 51 65 77 91 115 ,||, ll 173 1PPP—PTTDTTTTTTTTTTTTTT-44 I', ।, ill npe 11 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9972.D 050102.M Tue May 07 15:51:01 2002 Page 17

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