GCMS analysis results for sample AE10305, May 2002

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Laboratory report documenting gas chromatography-mass spectrometry analysis of environmental sample AE10305 conducted on May 17, 2002.

NYC-WTC_000045113–000045136

Folder label: “GCMS X 5/1/02 A 5/8/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\l\DATA\050802\10305R.D Vial: 26 Acq On 9 May 2002 12:56 pm Operator: Mclean Sample re-inj Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 8 Anthracene-dlO- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 23.11 0.51 ug/L 589078 Phenanthranene-dl0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dl0- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 87 3 2,2,9,9-Tetramethyldec-5-ene-3,7... 188 C14H20 102745-35-7 52 4 2-Quinolinecarboxaldehyde, 8-hyd... 188 C10H8N2O2 005603-22-5 36 Abundance Scan 3409 (23.109 min): 10305R.D (-3402) (-) m/z 188.10 100.00%| 188

5000

80 94 ..... 1..................... 1 1 i ' 1 1 1 1 1 ' 1 1 I 1 1 1 1 I 1 1 11 I 158 22.80 23.00 23.20 23.40 39 52 132 66 0 Tp 11111 'n TTTHl i" " i m/z 184.10 17.33%| m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

5000 1 1 I ' ' 22.80 23.00 23.20 23.40 m/z 189.10 16.91%| 80 94 leg 17 30 42 52 0 ,1 J 108118 132 146 1 170179/ — 0 ।' < ■ । । j 11 11 । i । [ I 11 i । 11 । । । 11 11 । i । 11 11 i I I i । । i r n [ t t-i t 11 । i r ] i 111 j'! i i i । 11 rl'l'i i i! । i । i । । I'l I m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188 ........ \ 1 1 i 1 ' 1 1 1 1-1 I ' 1 1 1 1 11 1 1 I 22.80 23.00 23.20 23.40 5000 m/ Z 94.05 16.39%I

80 94 160 30 42 52 66 11 108 118 132 146 || 170179,1,1 0 TTWTTTETTTTTTTTTHTH HH rill] 111 11 11 1111111 111 i rfl’r t j Trt । H'l p j 11 ] । । 11 [ ill n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79801:2,2,9,9-Tetramethyldec-5-ene-3,7-diyne I ' I I- I I I I I I " I j I I I 1 j I I-1 I [ 188 22.80 23.00 23.20 23.40 41 131 143 173 m/z 80.10 14.57%| 91 5000 77 158 57 119 27 67 105

0 -HHql+soal+ 44-4444—H T’t Tor i --- n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

10305R.D 050102 .M Thu May 09 13:51:06 2002 Page 11

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