GCMS analysis results for sample AE01638, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report . , Data File : C:\MSDCHEM\l\5973N\02FEB21\01638.D Vial: 7 Acq On : 21 Feb 2002 8:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 2-Propanol, 1-(2-methoxypro. . . Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 9.89 0.12 ug/L 60832 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxypropoxy)... 148 C7H16O3 013429-07-7 83 2 3-Heptanol (CAS) $$ 3-Hydroxyhep... 116 C7H160 000589-82-2 9 3 Butane, 1-ethoxy- 102 C6H140 000628-81-9 9 4 2,4-Pentanediol, 2-methyl- (CAS)... 118 C6H14O2 000107-41-5 9 Abundance Scan 577 (9.887 min): 01638.D (-) m/z 59.10 100.00% 59

5000

41 73 104 9.60 9.80 10.00 10.20

miz-> • • ।1 — i ■ • ‘ ■ i ■ ■ ' ■ i ■ ■ ■ ■ i ■ 0J- i ■ ■ " I ' " ■ l 20 30 40 50 60 70 80 .... 'I............... 90 100 110 120 130 m/z 41.10 16.92% Abundance #43942:2-Propanol, 1-(2-methoxypropoxy)- $$ 1-(2-Methoxyp... 59

5000 9.60 9.80 10.00 10.20 m/z 73.00 11.74% 31 45 --- ---------------- 73 104 130 0- miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #16988:3-Heptanol (CAS) $$ 3-Hydroxyheptane $$ 1-Ethyl-1-.. 41 59 69 Mr \ AD 31 9.60 9.80 10.00 lb'20 5000 87 m/z 43.10 11.41%

98 0- ■ ‘ i 1 ' ■ ■ i ' ''' I miz-> 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #9711: Butane, 1-ethoxy- 59 9.60 9.80 10.00 10.20 31 m/z 44.90 11.12% 5000

45 73 ,,,1,1,.,,, 1 87 102 i O—TT 1 ' 1 1 ' 111 1 1 1 TT ‘ i 11 •' i 1 1 11 I 11 ■ ■ i 1 ■ 1 ■ ■ ■ ' ■ i 1 1 ■ ■ i ■ '

miz—> 20 30 40 50 60 70 80 90 100 110 120 130 9.60 9.80 10.00 10.20

01638.D HP022102.M Mon Feb 25 10:55:50 2002 Page 7

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