GCMS analysis results for sample AE01638, March 2002

NYC 9/11 Public Portal Document Library Search Compound Report . . Data File : C:\MSDCHEM\1\5973N\02FEB21\01638.D Vial: 7 Acq On : 21 Feb 2002 8:11 pm Operator: Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 4 Acetic acid, 3-[1,3]dioxola... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 5.95 0.39 ug/L 196879 1,4-Dichlorobenzene-d4 9.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 42 2 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 42 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 25 4 Pentanol, 5-amino-__________________ 103 C5H13NO 002508-29-4 9 Abundance Scan 228 (5.948 min): 01638.D(-) m/z 73.10 100.00% 73

5000 43 ———————— 5.60 5.80 6.00 6.20 .............. .........11, 87 103 0- 111" " i111111 “ ■ i1' ■ • i ■ ′′′! ■ • ■ ■ i1 । . 111. । l I . , , i‘. . . t . . . , ।. . , . । . . . , । . . . . । , . . . । . , . , । . . . . ।. m/z 43.10 22.25% miz-> 10 20 30 40 50 60 70 80 100 110 120 130 140 150 160 170 180 ___ Abundance #78238: Acetic acid, 3[1,3]dioxolan-2-yipropyl ester 73

5000 —A 5.60 5.80 6.00 6.20 43 m/z 41.10 11.19% 5527 . , 87 113 174 0- f “ ” I ‘ ’ l Bapaduapanidp 'I.. ।. r. ।.... ।.... । .-i., ।.... ।..., ।। H .., ।.... ।. i.. ।, t

miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73 1 i 1 ■ ' ■ i 1 ■ ■ ' i ' ■ ■ ■ i 1 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.12% 43 27 87 0- mmpmn 55 .। i “ ■ • i “' 'il Hp 113 । • • • • i • > > • ।“ J• “ ’i “ “ i■'•■I “ ’* 1■’‘* 1 *’■’i • 174 miz-> 10 20 30 40 50 60 70 80 90 100 110 1Z) 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... ■ ' i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 ■ ■ ■ i ■ ■ ■ ■ i ■ 70 5.60 5.80 6.00 6.20 m/z 71.10 6.22% 5000

45 15 31 88 , 55. 0“i I . h i “ i “ ■ 'i ■ “11 ■ “ ■ i •" ■ i'11 ‘i' i ■1" i “ “ i ■ ■ “ i ■ ■ ■' i ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ I I l'i . । < ■ ■ i ■ • • 1 i ' ' ‘ i ■ ■ ■ • i ■ 1 ■ ■ i ‘ miz-> 10 2030405060 70 8090 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

01638.D HP022102.M Mon Feb 25 10:55:50 2002 Page 6

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