GCMS results for sample AE00321, Jan 24 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN11\00321.D Vial: 2 Acq On : 11 Jan 2002 2:57 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 11, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 2 (E)-1-Propenylaziridine $$ ... Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 4.85 0.17 ug/L 58750 1,4-Dichlorobenzene-d4 9.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 (E)-1-Propenylaziridine $$ Aziri... 83 C5H9N 080839-91-4 25 2 1-Hexene, 6-bromo- 162 C6HllBr 002695-47-8 17 3 1-Hexene, 6-bromo- 162 C6HllBr 002695-47-8 17 4 1-PROPENYL-AZIRIDINE 83 C5H9N 000000-00-0 10 Abundance Scan 129 (4.847 min): 00321 .D (-) m/ z 83.95 100.00% 84 55 41 5000 WWW

4.40 4.60 4.80 5.00 5.20 OPT ....... .................................... m/z 55.10 68.48% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #3037: (E)-1 -Propenylaziridine $$ Aziridine, 1-(1-propenyl... 41 55 83

. ......... ... 5000 27 4.40 4.60 4.80 5.00 5.20 68 m/z 59.10 60.43% 0 ' i11 TTTt -1 t i ' ■ • r i I'' i ■ ■ ■11 ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ■1 ■ ■ i ■1 ■111 ■ ■ ■ i1 ■ ■' i ■

n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #61497:1-Hexene, 6-bromo- 41 55 -44 ■ • A ■ i ' 1 ■

83 4.40 4.60 4.80 5.00 5.20 5000 27 m/ z 41.10 57.62% 67

n/z-> . mi 0 11'■'11'■ ■ 'I . .. 134 162 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 । 1' i ■1 ■ ■ i ■ ■ ■ ■ i ■ ■ ■' i ■ ■ ■ ■ i ■1 ■ ■ i ■ ■1 11'' ■ ■ i 11' ■ i ■

Abundance 41 5)5 #61496:1-Hexene, 6-bromo- 4.40 4.60 appppo, 4.80 5.00 5.20 m/z 83.10 53.46% 83 5000 27 67

' i ■ ■ ■ ■ i ■ ■ ■111 •' ■ i' ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ । . 136 162 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 4.40 4.60 4.80 5.00 5.20

00321.D SCAN508.M Mon Jan 14 10:46:42 2002 Page 4

NYC-WTC_000051401