GCMS analysis results for sample AE00833, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\02JAN31\00833.D Vial: 1 Acq On : 31 Jan 2002 2:42 pm Operator: Sample : 508 scan Inst : Instrumen Mise : January 31, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 3 2-t-Butyl-3-(1-methyletheny ... Concentration Rank 11

R.T. EstConc Area Relative to ISTD R.T. 4.63 0.04 ug/L 23374 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2 -t-Butyl-3 -(1-methylethenyl)oxa... 141 C8H15NO 000000-00-0 17 2 Hexane (CAS) $$ n-Hexane $$ Skel... 86 C6H14 000110-54-3 7 3 Hexane (CAS) $$ n-Hexane $$ Skel... 86 C6H14 000110-54-3 7 4 Cyclopropanecarboxylic acid (CAS... 86 C4H602 001759-53-1 7 Abundance Scan 110 (4.630 min): 00833. D (-) m/z 57.10 100.00% 57 88

41 5000

4.20 4.40 4.60 4.80 5.00 49 n/z-> O' । 20 ।।. TTTTT 30 40 50 60 70 80 .1............ 1 i ■ ■ ■ ' i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ' ' ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i

90 100 110 120 130 140 m/ z 88.10 92.69%

Abundance #37162: 2-t-Butyl-3-(1 -methylethenyl)oxaziridine 57

5000 41 85 4.20 4.40 4.60 4.80 5.00 "4 41.10 61.81% 70 O'. । .... । . PPPPPP in | Tr >1 ■ 11 ■ ■ ■ i • 11 ■ i. ■ ‘t’i .।।■ i. । 97 126 141 । /z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 N A Abundance #4248: Hexane (CAS) $$ n-Hexane $$ Skellysolve B $$ n-C6H1... 43 57

27 4.20 4.40 4.60 4.80 5.00 5000 m/z 85.10 44.88%

86

/z-> 0 1 i ' ' ‘I 1 ' ■ ' i 20 30 40 50 ■ ■ i ■ ■ 60 70 I140 80 90 100 110 120 130 Abundance #4237: Hexane (CAS) $$ n-Hexane $$ Skellysolve B $$ n-C6H1... । । ' > > । > । . . । i ■. 43 57 4.20 4.40 4.60 4.80 5.00 m/z 44.00 33.00%

5000

I W

86

m/z-> 0 20 30 37 40 „51 + 50 60 71 I '■i'■■■i 1 ■ 1 ■ i ' 1 ' ' i 1 ' ' 1 i ' 1 ' ' i ' ' ''i'1 ' ■ i ' ' ' ' i 70 80 90 100 110 120 130 140 4.20 4.40 II 4.60 4.80 ■R - 5.00

00833.D SCAN508.M Fri Feb 01 09:18:58 2002 Page 5

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