GCMS analysis results for sample AE00249, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C: \MSDCHEM\1\5973N\02JAN24\00249.D Vial: 5 Acq On : 24 Jan 2002 6:17 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 2 3-Buten-2-ol, 2-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

5.01 0.36 ug/L 152734 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 72 2 Butenol, methyl- 86 C5H10O 060766-00-9 64 3 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 59 4 3-Buten-2-ol, 2-methyl- (CAS) $$... 86 C5H10O 000115-18-4 56 Abundance Scan 143 (5.006 min): 00249.D (-) m/z 71.10 100.00% 43 71

5000 59 55 39 ' । ■1 4.60 4.80’ ' 5.00 5.20 5.40 ' i ■ ' ' ■ i ' ■ ■ ' i ‘ ■

miz—> 5 10 15 20253035404550556065 70 75 808590 7 51/ ir HM4 m/z 43.10 92.29% Abundance #4083:3-Buten-2-ol, 2-methyl- 7h 43 . , J 50001 IY.M0(o I MA PP 1 59 4.60 4.80 5.00 5.20 5.40 27 31 m/z 41.10 58.22% 53

iz—> 5 ■ ■11 ■ ■" i ■ ■ ■ ■ i ■1 ■ ■ i ■ "II 10 15 20253035404550556065 70 75 808580 —37 m H— Abundance #4093: Butenol, methyl- 43 7 -4-A44444444 4.60 4.80 5.00 5.20 5.40 5000 m/z 59.10 37.96% 59 27 15 31

mfa-> 5 “"i"" 331222317 10 15 20253035404550556065 70 75 808590 53 Hmpmp , 67, + Abundance #9384:2-Furanmethanol, tetrahydro- (CAS) $$ Tetrahydrofur... A 7h —A—4 4.60 4.80 5.00 • ■ ।' ■ ■ ■ । 5.20 5.40 ‘ ।1 ■

43 m/z 69.10 37.11%

5000 27 31

53 —

m/z—> —LA 1)" 37 > r) > i > >! ■ > ■ > p-> ■ >! > "II " ■ i111 ■ i1 5 10 15 20253035404550556065 70 75 808590 4,60 4.80 5.00 5.20 5.40

00249.D SCAN508.M Fri Jan 25 10:26:16 2002 Page 4

NYC-WTC_000050584