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GCMS analysis results for sample AE00276, Jan 2002

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Laboratory report showing GCMS analysis of sample AE00276 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051040–000051054

Folder label: “GCMS X 1/7/02 A 1/8/02

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\5973N\O2JANO8\276.D Vial: 1 Acq On : 8 Jan 2002 5:26 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L SU. ********************************************************************* Peak Number 3 3-Buten-2-ol, 2-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 5.01 0.22 ug/L 80862 1,4-Dichlorobenzene-d4 9.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 72 2 3-Buten-2-ol, 2-methyl- 86 C5H10O 000115-18-4 64 3 3-Buten-2-ol, 2-methyl- $$ .alph... 86 C5H10O 000115-18-4 64 4 2-Furanmethanol, tetrahydro- (CA... 102 C5H10O2 000097-99-4 53 Abundance Scan 143 (5.006 min): 276.D (-) m/z 71.10 100.00% 43 71

5000 55

207 A —Ar 4.60 4.80 ), . 1 1 11 i ' ,

5.00 5.20 5.40 0 "i""i l ‘TTTT m/ z 43.10 90.11% /z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #4083: 3-Buten-2-ol, 2-methyl- 71 43

5000 59 M N , ) w5.20AA5.40■ / 4.60 4.80 5.00 27 m/z 41.10 68.12% , 86 — 1W-rT]-rr+TyTTTTp-rTT o1 T TTTT-rp-ri-rp-rTTyTTTTp-rT^ n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210

N AW Abundance #4084: 3-Buten-2-ol, 2-methyl- 71 43 NAArAl) . / 4 60 4.80 5.00 5.20 5.40 5000 m/z 69.10 49.47% 59

27 86 0 . .. . -TTTTjTmpT1-r|TTTTpnTnp-rTTpTTTp-rTTpTTTpTTT^^ _l m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #4082: 3-Buten-2-ol, 2-methyl- $$ .alpha.,.alpha.-Dimethyl... - 71 4 60 4.80 5.00 5.20 5.40 m/z 55.00 35.12% 43 5000 59 27

miz-> 15/11... M— 0 " I" " I" " I" " I''" I 86 1"' i ’'1' i"'' i" " i" " i" " i" " r "' i" " i" " i" " I " ‘' i ■'1' I" " i" ' 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 5.20 5.40

276 .D SCAN508.M Wed Jan 09 15:16:16 2002 Page 5

NYC-WTC_000051048

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NYC-WTC_000051048Source: NYC Law Department, mirrored locally

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