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GCMS analysis results for sample AE00169, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.

NYC-WTC_000050519–000050538

Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02

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Scanned page image, NYC-WTC_000050536
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NYC 9/11 Public Portal Document 1 pMlit AM

Data File : C: \MSDCHEM\1\5973N\02JAN24\00169.D Vial: 2 • Acq On : 24 Jan 2002 3:48 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1... \SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 12 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 22.77 0.37 ug/L 287805 Phenanthrene-dl0 22.65

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 94 2 Anthracene-D10 188 C14D10 000000-00-0 93 3 Anthracene-dlO- 188 C14D10 001719-06-8 90 4 Acridine-D9_____ 188 C13D9N 000000-00-0 59 Abundance Scan 1699 (22.771 min): 00169. D (-) m/z 188.10 100.00% 188

5000 i | | i । i j i Pr > i i । i > i : । i 94 40 49 66 80 .. .. 160 2240 22.60 2280 23.00 23.20 mmmp-219 nalanns) m/z 94.05 19.46% nz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

........... / —?—mI 5000 ‘ I ‘ ‘ ‘ I ‘ 22.40 22.60 22.80 23.00 23.20 80 94 m/z 184.10 14.30% 66 , 158 — “ i “ ■ • i “ ‘11 “ 11111 TPmmmmmmpmp miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #84498: Anthracene-D1 0 188

22.40 22.60 22.80 23.00 23.20 5000 m/z80.00 11.31% 80 94 66 160 app i' “ ‘ I miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .......... ................................. Abundance #84502: Anthracene-d10- 188 2240 22.60 22.80 23.00 23.20 m/z 189.10 10.99%

5000

66 80 94 160 , I "।■■ ■■ । ' .. ...... I.... I......... ........ ,....,..,11..... . i ■' “ I ........... ) -PI ‘ I ‘ ‘ I ‘ n/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00 23.20

90169.D SCAN508.M Fri Jan 25 10:26:00 2002 Page 14

NYC-WTC_000050536

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NYC-WTC_000050536Source: NYC Law Department, mirrored locally

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