Laboratory report for sample AE00169 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
NYC-WTC_000050519–000050538Folder label: “GCMS X 1/4/02 A 1/24 - 1/25/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document JJcy DCatti ~Mpuia a\Sp J-
Data File : C:\MSDCHEM\1\5973N\02JAN24\00169.D Vial: 2 • Acq On : 24 Jan 2002 3:48 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 24, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 11 3-Cyanocarbazole $$ 9H-Carb... Concentration Rank 9
R.T. EstConc Area Relative to ISTD R.T.
22.28 0.15 ug/L 116109 Phenanthrene-dl0 22.65
Hit# of 5 Tentative ID MW Mol Form . CAS# Qual
1 3-Cyanocarbazole $$ 9H-Carbazole. .. 192 C13H8N2 057102-93-9 64 2 N-perdeuteriobenzylideneaniline 192 C13D11N 000538-51-2 64 3 Phenanthrene, 9-methyl- $$ 9-Met... 192 C15H12 000883-20-5 53 4 l-amino-2-methyl-4-isopropyl-thi... 192 C5H13N4PS 107264-54-0 50 Abundance Scan 1656 (22.280 min): 00169. D (-) m/z 192.10 100.00% 1912
5000
22 96 146 160 |. 22.00 22.20 22.40 22.60
m/z-> .111143.. 79.777 aa..... A IIF 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 • •i. “' i ■ ■"t 1 • i ■ m/z 191.10 15.89% Abundance #103424:3-Cyanocarbazole $$ 9H-Carbazole-3-carbonitrile (CAS 192
5000 22.00 22.20 22.40 22.60 164 m/z 146.10 15.45% 96 138 ■ ■ ■11 ■ ■ > ■ i ■' • ■ i ■ ■ • ■ i • ‘' • i' ‘1 ‘ i11 ■ • t11 -pmmTTTTTTT .• t •* * * i•"»r11 ‘ II |11 miz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #88409: N-perdeuteriobenzylideneaniline 192 A 22.00 22.20 22.40 22.60 5000 82 m/z 96.10 15.13%
54 110 30 94 160 mmmp • ■ i ■■ ‘ ■ i■ ■ ■ ■ i pHr— > • 111 m i j 1111 [ i j, > । • 11111 > > । j > 111 j i • i 111111 n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #103936: Phenanthrene, 9-methyl- $$ 9-Methylphenanthrene 192 22.00 22.20 22.40 22.60 m/z 193.10 14.99%
5000
96
n/z—> ........... 88,1 2′011101111911211111011101071017710177 139 152 165 176 Thpurt ■ i ■11 ■ i ’ ■ “ i “ ■ ■ i1 ■ ‘' i •■ ■ ■ i ■ ■ “ i' “11 ■ 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 U 22.00 22.20 22.40 22.60
30169.D SCAN508.M Fri Jan 25 10:26:00 2002 Page 13
NYC-WTC_000050535
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NYC-WTC_000050481
Laboratory report for sample AE00167 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050754
Laboratory report listing unknown compounds and surrogate recovery for sample AE00108 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050539
Laboratory report for sample AE00247 documenting detection of unknown compounds and surrogate recovery on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051967
GCMS analysis log for sample AE00739 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051930
GCMS analysis log for sample AE00737 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051895
GCMS analysis log for sample AE00702 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050683
Laboratory report listing unknown compounds and surrogate recovery for sample AE00166 analyzed on February 13, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050735
Laboratory report listing unknown compounds and surrogate recovery for sample AE00027 analyzed on February 7, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051877
GCMS analysis log for sample AE00701 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051860
GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000050596
Laboratory report listing unknown compounds and surrogate recovery for sample AE00250 analyzed on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000051586
Laboratory report showing GCMS analysis results for sample AE00613 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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NYC-WTC_000050432
Administrative record from DEP Box 28 documenting GCMS activities at the World Trade Center site in January 2002.
Filed in the same folder
NYC-WTC_000050433
Fragmented page containing a document identifier and instructions regarding liquid-liquid extractor drip rates from January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050435
Gas chromatography-mass spectrometry calibration analysis of sample AE00167 detecting multiple organic compounds including nitrosamines and dichlorobenzenes.
Filed in the same folder
NYC-WTC_000050439
Laboratory report listing concentrations of volatile organic compounds in sample AE00167 analyzed on January 24-25, 2002.
Filed in the same folder
NYC-WTC_000050444
Laboratory blank report for GCMS analysis of sample AE00167 showing compound concentrations and quality control values.
Filed in the same folder