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GCMS analysis results for sample AE01141, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.

NYC-WTC_000003543–000003562

Folder label: “GCMS X 1/20/02 A 2/25/02”

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Scanned page image, NYC-WTC_000003559
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Data File : C: \MSDCHEM\1\5973N\02FEB25\ 01141 .D Vial : 7 Acq On : 25 Feb 2002 4:11 pm Operator: . ’ Sample : 508 scan Inst : Instrumen Mise : February 2 5, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L Peak Number 11 DECADEUTEROPHENANTHRENE $$ ... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 22.77 0.58 ug/L 403812 Phenanthrene-dl0 22.63

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 DECADEUTEROPHENANTHRENE $$ Phena... 188 C14D10 001517-22-2 83 2 Acridine-D9 188 C13D9N 000000-00-0 80 3 Acridine-D9 188 C13D9N 000000-00-0 80 4 Anthracene-diO- 188 C14D10 001719-06-8 78 Abundance Scan 1718 (22.768 min): 01141 .D (-) m/z 188.10 100.00% 188

5000 -- 80 94

/z-> 42 52 01 ----- Pmmmmm --- 66 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 132 146 158 | . u 22.40 22.60 :22.80 23.00 m/ z 94.00 18.37%

Abundance #84500: DECADEUTEROPHENANTHRENE $$ Phenanthrene-d10 188

5000 22.40 22.60 22.80 23.00 80 94 m/z 80.00 16.92% 66 158

/z—> 0 TITTTIWWTTITTTTT TtT 40 50 60 70 80 ut ■11 ■ ■111'1 ■111''' ।11111'1111111H'1'' ।1 90 100 110 120 130 140 150 160 170 180 190 sslull. Abundance #85254: Acridine-D9 188 •........................... ‘ 1 1 ' ' ■ ' I • 1 1 1 1 1 1 1 1 1 1 22.40 22.60 22.80 23.00 5000 m/z 189.10 13.30%

93 158

n/z-> 0- m* 66 80 , 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 .... 4... 11

Abundance #85255: Acridine-D9 188 22.40 22.60 22.80 23.00 m/z 158.00 12.16%

5000

93 158 — 66 80 I 132 0 -H T1*TTTTIl m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.40 22.60 22.80 23.00

01141.D HP022102.M Tue Feb 26 08:30:27 2002 Page 13

NYC-WTC_000003559

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NYC-WTC_000003559Source: NYC Law Department, mirrored locally

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