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GCMS analysis results for sample AE01141, Feb 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE01141 conducted on February 27, 2002.

NYC-WTC_000003543–000003562

Folder label: “GCMS X 1/20/02 A 2/25/02”

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02FEB25\01141.D Vial: 7 Acq On : 25 Feb 2002 4:11 pm Operator: - Sample : 508 scan Inst : Instrumen Mise : February 25, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l-..\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 13 acrylic acid octadecanyl es... Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 28.50 0.44 ug/L 273811 Chrysene-dl2 30.49 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 acrylic acid octadecanyl ester $... 324 C21H40O2 004813-57-4 90 2 1-Docosene 308 C22H44 001599-67-3 70 3 acrylic acid hexadecanyl ester $... 296 C19H36O2 013402-02-3 68 4 acrylic acid tetradecanyl ester ... 268 C17H32O2 021643-42-5 64 Abundance Scan 2226 (28.503 min): 01141 .D (-) m/z 55.10 100.00% 55

5000 83 97 69 4' . ...... —........ 111 127 28.20 28.40 28.60 28.80 0- —Hl Ai ill ,141................................ ‘ • 1' I 11 ‘ ■ I ■ ' 1 ' 1 1 1 1 11 1 1 1 1 I ’ 11 1 11 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 ''ii1 m/z 57.00 54.23% m/z- > 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #275564: acrylic acid octadecanyl ester $$ 2-Propenoic aci... 55

5000 . ....... a. 83 28.20 28.40 28.60 28.80 97 70 m/2 83.10 52.94% 42 113127 IT I , IliI., I I II . .............. 0!1' ।11 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #259091:1 -Docosene 55 ..............................................

83 97 28.20 28.40 28.60 28.80 5000 m/z 43.10 46.66% 70 111 42 125 139 308 O-TTT i 1 11 ' i । ■ ■ i11'' ।1 ■] 11' ■ ■ ■ ।1 ■1 ‘ । ■ ■ ■1111 ■ ■ । ■1 ■111'1111111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #245493: acrylic acid hexadecanyl ester $$ 2-Propenoic aci... . ) A 55 28.20 28.40 28.60 28.80 m/z 73.00 46.44% 5000 69 42 I , . 97 111 127 O-T 1 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 28.20 28.40 28.60 28.80

01141.D HP022102.M Tue Feb 26 08:30:27 2002 Page 15

NYC-WTC_000003561

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NYC-WTC_000003561Source: NYC Law Department, mirrored locally

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