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GCMS results for sample AE00697, Jan 29 2002

Machine-extracted title · confidence 100%

GCMS analysis log for sample AE00697 showing surrogate recovery and unknown compounds detected on January 29, 2002.

NYC-WTC_000051860–000051876

Folder label: “GCMS X 1/10/02 A 1/16/02

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NYC 9/11 Public Portal Document

Data File : C:\MSDCHEM\1\5973N\02JAN16\00697.D Vial: 3 _ Acq On : 16 Jan 2002 12:31 pm Operator: Sample : 508scan Inst : Instrumen Mise : January 16, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\l..-\SCAN508.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N. L ********************************************************************* Peak Number 8 Eicosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 21.33 0.15 ug/L 84665 Phenanthrene-dl0 22.63 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Eicosane 282 C20H42 000112-95-8 90 2 Pentadecane $$ n-Pentadecane $$ ... 212 C15H32 000629-62-9 86 3 Eicosane 282 C20H42 000112-95-8 86 4 Nonadecane $$ n-Nonadecane 268 C19H40 000629-92-5 86 Abundance Scan 1573 (21.332 min): 00697.D (-) m/z 57.10 100.00% 57 71 43 5000 85

99 21.00 21.20 21.40 21.60

/z-> O-T 40 Ml 60 _1 80 100 120 140 160 180 200 220 240 260 280 m/z 71.10 64.95% Abundance #228992: Eicosane 43 57

5000 71

85 ....... A. 21.00 21.20 21.40 21.60 m/z 43.10 59.09%

m/z-> , , II OPT "Imu 40 60 411 127 14122 80 100 120 140 160 180 200 220 240 260 280 Abundance #134011: Pentadecane $$ n-Pentadecane $$ CH3(CH2)13CH3 57 43 x A 71 21.00 21.20 21.40 21.60 5000 m/z 85.10 39.94% 85

n/z-> O-T 40 J60TTr 80 100 41^3,1?1 155 169 , 212 120 140 160 180 200 220 240 260 280 Abundance #228988: Eicosane ........ . 57 21.00 21.20 21.40 21.60 43 m/ z 41.10 27.47% 71 5000 85

99 0' ' P T TTr LX I 113 127 141 155 169 -------- 282 1 ■ | 1 • • ■ i k ■ ' ■ I ' ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 21.00 21.20 21.40 21.60

J0697.D SCAN508.M Thu Jan 17 08:16:56 2002 Page 10

NYC-WTC_000051873

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NYC-WTC_000051873Source: NYC Law Department, mirrored locally

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