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GCMS analysis results for sample AE00318, Jan 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00318 for unknown compounds and DDD on January 10, 2002.

NYC-WTC_000051105–000051121

Folder label: “GCMS X 1/7/02 A 1/8/02

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Scanned page image, NYC-WTC_000051115
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\MSDCHEM\1\5973N\O2JANO8\318.D Vial: 3 Acq On 8 J an 2002 7:06 pm Operator: Sample 508scan Inst : Instrumen Mise January 8, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508 .M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L

Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 5.89 4.11 ug/L 1401180 1,4-Dichlorobenzene-d4 9.72

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6(33/ 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 Silane, tetramethyl- $$ Tetramet... 88 C4H12Si 000075-76-3 28 4 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 Abundance Scan 220 (5.885 min): 318. D (-) m/z 73.10 100.00% 73

5000 43

W 5.60 5.80 6.00 6.20

n/z-> ml 55 . . 87 1 ‘‘ ' ,, ‘ 000 01 • I • ■ ■ • I ■ 103 m/z 43.10 24.70% 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 70

5000 5.60 5.80 6.00 6.20 43 m/z 45.10 9.79% 27 ... 5555 87 113 174 0^ TEmTT +T— Tuuuuua** TTTTT ...... ............. /z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 70 1 ' ■ ■ i • TTT 5.60 5.80 6.00 6.20 5000 m/ z 41.10 9.09% 43 27 55 , 8/ 113 174 0-TTTTT ' i " " I " 1' i' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #4812: Silane, tetramethyl- $$ Tetramethylsilane $$ (CH3)4... .11 Am . 1 . 70 5.60 5.80 6.00 6.20 m/z 71.10 6.71%

5000

45 31 15 | 55 | 88 0 TTUTMHgTmp lasg*sttyksssn"sssussdsA*dddd288*4****0*********|*I| m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 1 50 160 170 180 5.60 5.80 6.00 6.20

318.D SCAN508.M Wed Jan 09 15:17:41 2002 Page 7

NYC-WTC_000051115

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NYC-WTC_000051115Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.994

machine-extracted · confidence unavailable · Check page ↗

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