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← Document results/DEP Box 28/GCMS X 1/8/02 A 1/10/02
Document / 17 pages

GCMS results for sample AE00471, Jan 18 2002

Machine-extracted title · confidence 100%

Laboratory report showing GCMS analysis of sample AE00471 with surrogate recovery data on January 18, 2002.

NYC-WTC_000051301–000051317

Folder label: “GCMS X 1/8/02 A 1/10/02”

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Scanned page image, NYC-WTC_000051311
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \MSDCHEM\1\5973N\02JAN10\00471.D Vial : 6 Acq On : 10 Jan 2002 6:57 pm Operator: Sample : 508 scan ext 1/8 Inst : Instrumen Mise : January 10, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\SCAN508. M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.89 5.24 ug/L 1717170 1,4-Dichlorobenzene-d4 9.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 33 2 Acetic acid, 3 -[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 33 3 N-Ethylformamide $$ N-Formylethy... 73 C3H7NO 000627-45-2 9 4 Butane, 2-methoxy-2-methyl- $$ E... 102 C6H140 000994-05-8 9 Abundance Scan 220 (5.885 min): 00471 .D (-) m/z 73.10 100.00% 7)3

5000 43 .ve)) p n । . . . . 5.60 5.80 6 00 6.20 0TTTTPTTTTTTTTTTTTT ■ ‘ ‘11 ... 87.... 103..................... .11 55 I’’’ ' I' ■' ‘ I''' • I'''' I •''11'''' I' ■' 11'1'' I' TITT m/z 43.10 24.82% n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180

N Abundance #36138: 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73

5000 5.60 5.80 6.00 6.20 43 m/z 41.10 9.35% 27 55 । 87 113 174 0-p TT 1’’1“tuum—uuumuu*)unu—00’00OTT m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 #78238: Acetic acid, 3-[1,3)dioxolan-2-ylpropyl ester 73 .... A____ 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.25%

43 27 55 , 87 113 174 01 ' r ' " i' " ' r TTTI4 ■ i " " i " ' ‘I’ 1'' i " 1' i " " i " '' i " 111" 111" I" " I " " r ' " i " r 11' m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... 1/ p । > । । । । । 30 5.60 5.80 6 00 6.20 73 m/z 71.10 6.37%

5000 __ 44 58

/z-> 0 TTI" 15 rir II H TCII*umuu]DOTNTTTTTTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 5.60 5.80 6.00 6.20

)0471.D SCAN508.M Fri Jan 11- 10:08:50 2002 Page 7

NYC-WTC_00005131 1

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NYC-WTC_000051311Source: NYC Law Department, mirrored locally

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DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004494

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗
DEP GCMS data table, Jan-Feb 2002 · Box DEP Box 12

NYC-WTC_000004935

Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

1 shared non-person entities · 1 shared topics · similarity 0.995

machine-extracted · confidence unavailable · Check page ↗

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