GCMS analysis report for sample AE01510, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report . Data File : C: \MSDCHEM\1\5973N\02FEB21\01510.D Vial: 5 Acq On : 21 Feb 2002 2:17 pm Operator: • Sample : 508 scan Inst : Instrumen Mise : February 21, 2002 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\MSDCHEM\1...\HP022102.M (RTE Integrator) Title : 508 scan method Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 5 3-(CYCLOHEX-3'-EN-YL)PROPAN... Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

5.95 0.53 ug/L 240299 1,4-Dichlorobenzene-d4 9.72

Hit# of 5 Tentative ID MW Mol Form CAS# Qual 1 3-(CYCLOHEX-3'-EN-YL)PROPANOL $$... 174 C8H14O4 015745-87-6 36 2 Acetic acid, 3-[1,3]dioxolan-2-y... 174 C8H14O4 000000-00-0 36 3 N-Ethylformamide $$ N-Formylethy. . . 73 C3H7NO 000627-45-2 9 4 Propane, 2-methoxy-2-methyl- (CA... 88 C5H120 001634-04-4 9 Abundance Scan 228 (5.948 min): 01510.D (-) m/z 73.00 100.00% 73

5000 43 55 5.60 5.80 6.00 6.20 01.»।' 11 > 11 >' > । ■ — 1} , 87 103 m/z 43.10 24.31% T' CITB ‘ 111 'I i i I i ! l'i | | . . . I . . ! . . . . I. . I . ! 1 i . . I . . . . I . . . I I. . . . I I .. . । . iz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #36138:3-(CYCLOHEX-3'-EN-YL)PROPANOL $$ 2-Cyclohexene-1-p... 73.

5000 —PPTPI TTBorr" 5.60 5.80 6.00 6.20 N V

43 m/z 41.10 10.64% 27 87 113 174 0-mpp • i •55 • i • • • ■ ,i।. +pr ' i'‘i ■ ‘ ■ ■ i “ ■ ■ r ■ i" “ । ■' • ■ । । i ■" • i •' “ । ■ m/z—> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 Abundance #78238: Acetic acid, 3-[1,3]dioxolan-2-ylpropyl ester 73 ■ 1 i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ‘ 1 i ■ ■ ■ ' । 1 5.60 5.80 6.00 6.20 5000 m/z 45.10 9.41% 43 27 87 113 174 0- Tptt 55 । 11 ‘11 ■ i1 “ ■ i' I.. ।.> 1111 >.11111 < । ri< 11 •i.. ।.. । >111 ■> ।. ।. 11.।. । > i..।. m/z-> 10 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 150 160 170 180 Abundance #1794: N-Ethylformamide $$ N-Formylethylamine $$ Formamide... A A 30 5.60 5.80 6.00 6.20 73 m/z 71.00 5.93% 5000 44 58

n/z—> 0 . 15 pdaguak. -H TT 111’I1! III 11 M I I 111 111 I 11 n ■

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 I T| rr 11 11 i 11 । i 11 i [ > t 11 ।, i n | j ■ ■ । ‘ 5.60 । 5.80 z • f‘ ‘ 6.00 । ■ ■ ■ ■ ।1 6.20

01510.D HP022102.M Mon Feb 25 10:55:10 2002 Page 7

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