GCMS results for sample AE07766, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\07766.D Vial: 28 Acq On : 16 Apr 2002 8:51 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 16 Formamide, N-(cyanomethyl)- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

31.50 0.29 ug/L 296650 Chrysene-dl2 30.88

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Formamide, N-(cyanomethyl)- 84 C3H4N20 005018-27-9 9 2 Acetic acid, 2-(l-buten-3-yl)-2-. 187 C8H13NO4 1000159-09-9 9 3 Ethanone, 1-cyclopropyl-, oxime 99 C5H9NO 1000221-89-7 7 4 2H-Pyran, 2-(3-butynyloxy)tetrah. .. 154 C9H14O2 040365-61-5 4 Abundance 40 Scan 4837 (31 499 min): 07766.D (-4833) (-) m/2,42:20100,00% 5000 84 55 99 113 71 TF 31 20 31.40 31.60 31.80 I 240 01 mPT 44.87% n/z-> 20 40 80 100 120 140 160 180 200 220 240 Abundance #541' Formamide, N-(cyanomethyl)- 29 M1 84 55 5000 31.20 31.40 31 60 31.80 40 m/z 99.30 37.64% 0— . । H illt j. 11 l' 66 1■। 1 1 i 1 m/z—> 20 40 60 80 100 120 140 160 180 200 220 240 Abundance #393: Acetic acid, 2-(1-buten-3-yl)-2-nitro-. ethyl ester 29 4 - 1 I 1 11 1 I 1 ' 31 20 31 40 31.60 31.80 41 55 m/ z 35.17% 5000 67 83 95 90 112

n/z- > ov 41nl4lqqlu,l 20 40 60 80 100 .120, 129 140 140.157.172 160 180 ....200........... 220 240 . Abundance #1242. Ethanone, 1-cyclopropyl-, oxime 39 31 20 31.40 31 60 31 80 m/z 55.30 32.89% 5000 27 55 67 82 98 wmhu/"astuks. T)/Z—> 0 — LL— 20 40 60 80 Pu I ' T 100 120 140 160 180 200 220 240 1 ' i ' TB" 31 20 31 40 31 60 31.80

07766.D 041202SCAN.M Tue Apr 16 13:42:18 2002 Page 19

NYC-WTC_000046887