GCMS analysis results for sample AE11422, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\052002\11422.D Vial: 12 Acq On : 20 May 2002 10:14 pm Operator: Mclean Sample : 5/16 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 7 Phenanthrene-dlO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.41 ug/L 324724 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene-dlO 188 C14D10 001517-22-2 81 2 Anthracene-dlO- 188 C14D10 001719-06-8 81 3 3-Amino-4-methyl-6-methoxyquinoline 188 C11H12N2O 1000213-71-3 40 4 4-Methyl-2-(4-fluorophenyl)pyrim... 188 C11H9FN2 076128-67-1 38 Abundance Scan 3408 (23.103 min): 11422.D (-3402) (-) m/z 188.10 100.00% US

5000

80 94 158 22.80 23.00 23.20 23.40 44 66 0- ।' i ■ ■ । ■ ■ ■ ■ ।" ।111 ‘1111"1111 ■' । 11' ’' I'11 ‘ ] "T m/z 94.05 21.02% miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 its

- 5000 22.80 23.00 23.20 23.40 80 m/z 184.10 17.68% 94 160 30 42 52 66 11 108 118 132 146 II, 170179.1,1 0 TDTRTTTTT 1 rti . . । l l i , r rl I , ] i . 14 1. rt )■TT mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d 10- 148

22.80 23.00 23.20 23.40 5000 m/z 80.05 16.39%

80 94 160 66 17 30 42 52 0 ' i " " i " " I " " 11' " i111 -HH++108.118..132.146—170179— mlz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79771:3-Amino-4-methyl-6-methoxyquinoline 188 22.80 23.00 23.20 23.40 m/z 158.00 13.83% 145 5000

117 159 173 m/z—> 0- 41 51 63 77 89 102 ------------ 130

10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 IP ..................... .......................... 22.80 23.00 23.20 23.40

11422.D 050102.M Thu May 23 10:49:14 2002 Page 9

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