GCMS results for sample AE08070, Apr 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\020415\08070.D Vial: 27 Acq On : 16 Apr 2002 8:02 am Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method C:\MSDCHEM\1\METHODS\041202SCAN.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98.L Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

5.96 0.43 ug/L 275823 1,4-Dichlorobenzene-d4 9.99 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 9 3 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 4 Acetic acid, 3- [1,3]dioxolan-2-y. . . 174 C8H14O4 1000186-02-3 9 Abundance Scan 490 (5 958 min) 08070 D (-485) (-) m/z 73.30 100.00% 73

5000

43 / 55 5 60 5 80 6 00 6 20 6 40 87 103 01 ------- i , .i i h 1 ' ‘1 I ■ 1 1 ■ I । ‘ । 1 I ■ m/ z 43.30 23.73% Ti/Z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #857: N-Ethylformamide 33 73

5000 58 5 60 5.80 6.00 6.20 6.40 44 m/ z 41.30 9.14% 18

n/z— > 0 181,1/25 10 20 4344 30 40 — 50 60 70 80 i ' ■ ' ■ i' 1 ' i । ■ ■ ■ ■ । ■ ■ ■ ■ । ' । । 90 100 । । । 110 Abundance #114875' 3-Pentanol, 3-methyl- 73 560 5.80 6 00 6 20 6 40 5000 m/ Z 45.30 8.93% 55 27 45 87 0- 15 ■ ■ i ■ ■' ■ 1 । ■ 1,132। । 39 1| 50 —flu I. * * i 1 ' i ........... ..... Tl/Z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #254 72. Pentane, 3-methoxy- 73 5 60 5.80 6 00 6.20 6.40

5000 45

Tl/Z—> 0 10 —1 20 30 40 50 55 ■ । 50 ■ ■ 1 1 । " " 60 674++ 70 ............................... 101 80 90 100 110 5.60 5.80 6 00 6.20 6.40

08070.D 041202SCAN.M Tue Apr 16 13:58:50 2002 Page 3

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