GCMS surrogate recovery report, sample AE12763, June 2002

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Data File : C:\MSDCHEM\l\DATA\061102\12763.D Vial: 7 Acq On : 11 Jun 2002 2:46 pm . Operator: Sample : re-ext. Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C: \DATABASE\NIST98 . L ********************************************************************* Peak Number 16 Anthracene, 9-methyl- Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

22.53 0.32 ug/L 392657 Phenanthranene-dl0 22.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Ant hracene, 9 - methyl- 192 C15H12 000779-02-2 50 2 2,5-Dihydrophosphole, 3-methyl-l... 192 C11H13OP 1000196-97-5 45 3 Anthracene, 2-methyl- 192 C15H12 000613-12-7 42 4 Phenanthrene, 9-methyl-____________ 192 C15H12 000883-20-5 42 Abundance 7 Scan 3311 (22.533 min): 12763.D (-3305) (-) m/z 192.00 100.00% 192

5000

96 146 42 51 70 82 Of-i “ " i ■ TTHHT ‘ITT 120 mH 160 ............................................................. z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 l 22.20 22.40 22.60 22.80 m/z 191.00 21.52% Abundance #125849: Anthracene, 9-methyl- 192

................. I................. । ■ ... । 5000 22.20 22.40 22.60 22.80 m/z 96.10 16.07% 96 165 28 39 51 63 74 83 J 105 115 126 139 152 , 176 n 01 —LmPTTTTTTTTTmTTTTTTHm 'tTTTTT miz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965:2,5-Dihydrophosphole, 3-methyl-1-oxo-1 -phenyl- 192 164 22.20 22.40 22.60 22.80 5000 99 m/z 193.10 15.02% 115 47 77 177 67 125,2 146 27 38, 157+87 0 1111 “1111 ’!“ 1,48174,455,. +f m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #125844: Anthracene, 2-methyl- 192 22.20 22.40 22.60 22.80 m/z 146.00 14.34%

5000

93 96 165 0 .............. 63 74 33, . ... 115 139 150 , 176 ‘ I " " I" ' ’ IH‘ I ‘ Th’ 4-rrp-r m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80

12763.D 060302.M Tue Jun 11 15:54:17 2002 Page 19

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