GCMS surrogate recovery report, sample AE12763, June 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\061102\12763.D Vial: 7 Acq On : 11 Jun 2002 2:46 pm Operator: Sample : re-ext. Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\060302.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 17 Anthracene-dlO- Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 23.06 0.40 ug/L 486730 Phenanthranene-dl0 22.91 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Anthracene-d/o- 7 188 C14D10 001719-06-8/94 2 Phenanthrene-diO 188 C14D10 001517-22-2 90 3 Cycloheptanone, 4-phenyl- 188 C13H160 067688-28-2 47 4 Selenide,/ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 42 Abundance Scan 3401 (23.062 min): 12763.D (-3392) (-) m/z 188.10 100.00% 188

5000 .................... ......................... 04 158 .........43/57 66 80... 0 > । << < , । i ,, | 11 11 | 1'q > i 146 ,|| j 11 11 |'i ■ f 111 I I I |'I I 11 i i • • i • • ■ ■ i * * • * i" * * i • *1 • i * * I i | * ■" । * ‘I 22.80 23.00 23.20 23.40 m/Z94.00 16.86% mfe-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- US

5000 22.80 23.00 23.20 23.40 m/z 189.10 15.47%| e 80 94- 160 . 17 30 42 52 ° , , 108118 132 146 ,|I 17017911 0- 111 n | n n | n n 111 ii j I! 11{ 111 11 i I 11 11 j 1111111 rt 111 nj n 11 |'l 111 । u 11 |i! "ITrt tin ini| miz-> 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

22.80 23.00 23.20 23.40 5000 m/z 184.05 13.89%|

80 94 160 30 42 52 66 n/z-> 0 ‘1 'I 1 11 1 I ""I' ' " |'l " | H l' | “ 11 . || hT 108118 132 146 n. 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 1701791.. Abundance #79739: Cycloheptanone, 4-pheny- 188 22.80 23.00 23.20 23.40 117 m/z 158.10 11.17%| 104 91 160 5000 131 170 27 39 51 65 145 -444 i 78 0- +lHH Hl ‘T‘11 m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 22.80 23.00 23.20 23.40

12763.D 060302.M Tue Jun 11 15:54:19 2002 Page 20

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