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GCMS analysis results, sample AE09155, May 2002

Machine-extracted title · confidence 100%

GCMS analytical report for environmental sample AE09155 including surrogate compound data from May 15, 2002.

NYC-WTC_000022857–000022878

Folder label: “GCMS X 5/8/02 A 5/10/02

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Scanned page image, NYC-WTC_000022869
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\MSDCHEM\1\DATA\050902\9155.D Vial: 20 Acq On : 10 May 2002 7:36 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 5 Anthracene-diO- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.36 ug/L 408881 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-diO- 188 C14D10 001719-06-8 90 2 Phenanthrene-diO 188 C14D10 001517-22-2 87 3 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 50 4 1,3,5-Triazin-2-amine, 4,6-bis(m... 188 C5H8N4S2 030358-19-1 43 Abundance Scan 3408 (23.103 min): 9155.D (-3403) (-) m/z 188.10 100.00% 188

5000 ----- 80 94 158 22.80 23.00 23.20 23.40 43 66 0 mmmprH .■ill........... 12...... Il)....... , m/z 94.00 16.10% mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d 10- 1t8

5000 22.80 23.00 23.20 23.40 m/ z 80.10 14.27% 80 94 160 66 17 30 42 52 , 108118 132 146 ,|| 170179.1 0 —PmHr iguik — H | I I > ■ | ■ I . | n I 1 | n . > IT. I . | I . | rTr I I I | I I I I | I’l miz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 1tS ........... ......................................... 22.80 23.00 23.20 23.40 5000 m/z 189.15 13.70%

80 94 160 30 42 52 66 m/z-> 1 108118 132 0 TmPPTTTTTTTH I I । । [ ' । I I [ I i n | i 111 ■11 j - "i i ■ ‘-r 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 146 , 1.179179... Abundance #79821: Selenide, ethyl 1-methyl-1-penten-3-ynyl .........) T-T-p-T^- 1 1 I ' 1 ' ‘ 1 ' * 1 ' I 188 22.80 23.00 23.20 23.40 m/z 158.20 12.28%

5000 79 159

m/z—> m0 91 -4 107 119 131 145 । TTTTTTTTTTTTTTTTTTTTTTTTT 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 173 -rm-|

22.80 23.00 23.20 23.40

9155.D 050102.M Mon May 13 11:41:47 2002 Page 8

NYC-WTC_000022869

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NYC-WTC_000022869Source: NYC Law Department, mirrored locally

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