NYC-WTC_000023904
Laboratory report showing GC/MS analysis of sample AE10981 with surrogate recovery data for 2,4-DDD.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Document / 22 pages
GCMS analysis results, sample AE09155, May 2002
Machine-extracted title · confidence 100%GCMS analytical report for environmental sample AE09155 including surrogate compound data from May 15, 2002.
NYC-WTC_000022857–000022878Folder label: “GCMS X 5/8/02 A 5/10/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\MSDCHEM\1\DATA\050902\9155.D Vial: 20 Acq On : 10 May 2002 7:36 am Operator: Mclean Sample : 5/8 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHCDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 4 3-(2-Methoxy-5-methylphenyl... Concentration Rank 12
R.T. EstConc Area Relative to ISTD R.T.
22.58 0.29 ug/L 327507 Phenanthranene-dl0 22.95
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H1203 103986-76-1 53 2 Thiophene, 2-[2-(3-thienyl)ethen... 192 C10H8S2 116854-09-2/50 3 2-Propenal, 3-(3,4-dimethoxyphen... 192 C11H1203 004497-40-8 42 4 Coumarin-7,8-diol 192 C1OH804 1000129-31-6 38 Abundance Scan 3319 (22.580 min): 9155.D (-3311) (-) m/z 192.10 100.00% 192
5000 ........................ 96
miz-> 42 66 OlTTTTTTTTTTTT TTTTTTTTTTTTT 82 120 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 m II 146 160 22.20 22.40 22.60 22.80 23.00 m/Z 191.10 22.43%
Abundance #80954:3-(2-Methoxy-5-methylphenyl)acrylic acid 161 192
----- 5000 105 22.20 22.40 22.60 22.80 23.00 n 132 m/z 193.10 18.41% 91 115 , 145 39 51 65 । 175 miz-> 0 ■ i' “1 r ----- -JiUmHH+ -1’11’1 Tur 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #81023: Thiophene, 2-[2-(3-thienyl)ethenyl]- 192
147 22.20 22.40 22.60 22.80 23.00 5000 m/ Z 96.00 17.54% 45 58 69 96 115 158 , 134 177 27 0- TITTTTT -++44+4+++195—H— — ■ i ■i ■ ■ '11" m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- ‘ I ' ' 1 1 1 1 ' 1 1 I ' ' . 192 22.20 22.40 22.60 22.80 23.00 161 m/z 146.00 17.21%
5000 77 121 149 177 91 103 52 64 138 - .....I ,... 0 ’ * ’14 Tp m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00
9155.D 050102 .M Mon May 13 11:41:46 2002 Page 7
NYC-WTC_000022868
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NYC-WTC_000022868Source: NYC Law Department, mirrored locally
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