GCMS analysis results, sample AE09155, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\050902\9155.D Vial: 20 Acq On : 10 May 2002 7:36 am Operator: Mclean Sample : 5/8 eh Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 3 2-Pentanone, 4-hydroxy-4-me... Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 5.97 12.92 ug/L 10654600 1,4-Dichlorobenzene-d4 9.93

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanone, 4 -hydroxy-4-methyl- 116 C6H1202 000123-42-2 86 2 2-Pentanone, 4 -hydroxy-4 -methyl- 116 C6H1202 000123-42-272 3 2-Pentanone, 4 -hydroxy-4 -methyl- 116 C6H1202 000123-42-2 59 4 Acetic acid, 1,1-dimethylethyl e... 116 C6H1202 000540-88-5 36 Abundance Scan 491 (5.964 min): 9155.D (-485) (-) m/z 43.10 100.00% 43

5000 59

101 .__ K___ 560 5.80 6.00 6.20 6.40 37 i, 53 69 83 , | 117 125 01 ............................. 1 ■ I । i 1 1 I । । 1 । । 1 ' 1 ( I1 In । । T i'l f j ■ > ■ ■ । ■ ■ ■ ■ । । ■ l ■ 1 m/z 59.10 36.96% m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #109755:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 59 5.60 5.80 6.00 6.20 6.40 m/z 58.10 20.70% 15 101

n/z-> Of ■ ■ i 1 10 X20,25131/37,1 30 40 53, TTTTT 50 60 70 80 ............ 83........... j ............................... 90 100 110 120 130 Abundance #109756:2-Pentanone, 4-hydroxy-4-methyl- 43 560 5.80 6.00 6.20 6.40 5000 59 m/z 101.10 13.98%

83 . 92 93 101 n/z- > 0) ..101—20 25.3144 30 71 40 50 60 70 । ' । । 1 1 ' । 1 1 1 1 I... I***I‘‘‘‘I* 80 । " i ’ ''i I ■ ' 1 ■ i ■ 90 100 110 120 130 Abundance #5851:2-Pentanone, 4-hydroxy-4-methyl- ■ ' i ■ ■ ■ ■ i ■ ' 43 5.60 5.80 6.00 6.20 6.40 m/ z 41.20 6.07%

5000 59 . 101 0 0 27 1 /1 37 Yll i'' 1 53 67 77 | 83‘ ' ■ 91 । | 1 ■ ' ■ | । , | ! ■ ■ ' 1 j l ■ ' ■ j 1 ' 1 ' i ■ ' 1 ■ | ■ Tr—pTRTTrRTTrr n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 5.60 5.80 6.00 6.20 6.40

9155.D 050102.M Mon May 13 11:41:46 2002 Page 6

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