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GCMS analysis results for unknown compounds, sample AE10198, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE10198 on May 10, 2002.

NYC-WTC_000044885–000044901

Folder label: “GCMS X 4/30/02 A 5/8/02”

←Page 13 of 17→
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\10198.D Vial: 16 Acq On 9 May 2002 3:38 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title 508 Modified GC/MS scan Library C:\DATABASE\NIST98. L ********************************************************************* Peak Number 5 3 -(2-Methoxy-5-methylphenyl .. . Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

22.58 0.32 ug/L 432517 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-(2-Methoxy-5-methylphenyl)acry... 192 C11H12O3 103986-76-1 5 2 Bitoscanate 192 C8H4N2S2 32 004044-65-9 P 3 Thiocyanic acid, 2-benzothiazoly... 192 C8H4N2S2 006011-99-0 50 4 1,5-Naphthalenedithiole 192 C10H8S2 1000223- -5 45 Abundance Scan 3319 (22.580 min): 10198.D (-3304) (-) m/z 192.10 TOO.00% 192

5000

146 160 m m/z-> 40 54 — 82 ,70 96 11, 0 [ I ,! I | I >! I | ! I <■ | I I I > [ I I I I | I I ! I | I I I' 1 | 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 118 TPTT L i111' i 22.20 22.40 22.60 22.80 23.00 m/z 191.00 19.79% Abundance #80954: 3-(2-Methoxy-5-methylphenyl)acrylic acid 161 192

5000 105 22.20 22.40 22.60 22.80 23.00 77 132 m/z 193.10 13.41% 91 115 , 145

m/z-> 0 39 l ,444423.1— 4 .... bijar । l — 51 65 1 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 , 175 I’i 1 ■ 1 ■1111'11' I

Abundance #125828: Bitoscanate 192 1 1 1 I ' ' ' 1 I ' 22.20 22.40 22.60 22.80 23.00 5000 m/z 146.10 13.17% ft 134 90 160 40 50 63 75 Y W2 122 148 0 ------------------ 1TH 176 m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80870: Thiocyanic acid, 2-benzothiazolyl ester 192 1 4 22.20 22.40 22.60 22.80 23.00 m/Z 82.00 10.95%

5000

134 45 “f 82 90 ( 108 122; | 148 160 ! ,.. A. .. OT - । rri P J ri > | i । I > । I । > | । । I > । । । I ।‘ । । TPT m/z-> 30 40 50 ! 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

10198.D 050102.M Thu May 09 13:35:24 2002 Page 8

NYC-WTC_000044897

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NYC-WTC_000044897Source: NYC Law Department, mirrored locally

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1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997

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