GCMS analysis results for unknown compounds, sample AE09093, May 2002

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Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE09093 on May 10, 2002.

NYC-WTC_000044902–000044925

Folder label: “GCMS X 4/30/02 A 5/8/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\9093 .D Vial : 15 Acq On 9 May 2002 2:49 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\l\METHQDS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ****************************************************************** * * * Peak Number 7 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

23.11 0.55 ug/L 761436 Phenanthranene-dl0 22.95

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 91 2 2 Phenanthrene-dlO 188 C14D10 001517-22-2 87 3 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 59 4 4-Methyl-2-(3-fluorophenyl)pyrim... 188 C11H9FN2 076128-66-0 50 Abundance Scan 3409 (23.109 min): 9093.D (-3403) (-) m/z 188.10 100.00% 108

5000 ........ Til I 1 / I 1 ......................... I I I I I I I 1//l/l/m/k— I I f 80 94 22.80 23.00 23.20 23.40 42 54 66 132 '11'1111111' i11111''111 TTH 146 158 m/z 189.15 13.48% 0 i I til r I 111 I I I I I I "i > t 111 I II I I I I I 111 I I I I 1" r 11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79826: Anthracene-d10- 188

.......... ............................. 5000 22.80 23.00 23.20 23.40 m/z 80.10 13.25% 80 94 160 , I 66

m/z-> 17 30 42 52 , . | 108 118 132 0 I I I I I I I I i I I I I I I I [ I I I I I I I I I | I I I I | I I I I | I I I trrttr I I I I | I U I | I । I 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 146—4179179 4— Abundance #79827: Phenanthrene-d10 188 ' 1 i 1 111*1 ""I 22.80 23.00 23.20 23.40 5000 m/ z 184.05 12.89%

80 94 160 66 0- 111111 30 42 52 111 rt 11111111 it 11111111111 108 118 132 146 illlliiriilliltilril.fi ITETTT .i 1791794 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79821: Selenide, ethyl 1-methyl-1-penten-3-ynyl ........ Til l I /I ............................. I I I [ I I I [ I I I B I I I [ 188 22.80 23.00 23.20 23.40 m/z 94.10 11.57%

5000 79 . 159 145 173 0 ...........I r 11' I u TI— Wr 91 107 119 131 I I I I I I I 1 I I I I I I I I I I I I I I I t I I I I I I r I I I I —"‘m 111 Tr l I I I > J I I —i I I I I I I I I I I I I

m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 22.80 23.00 23.20 23.40

9093.D 050102.M Thu May 09 13:33:30 2002 Page 10

NYC-WTC_000044916

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GCMS analysis results, sample AE09973, May 2002 · Box DEP Box 25

NYC-WTC_000044025

Laboratory report for sample AE09973 showing surrogate recovery and unknown compounds from May 9, 2002.

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