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GCMS analysis results for unknown compounds, sample AE09093, May 2002

Machine-extracted title · confidence 95%

Laboratory report showing gas chromatography-mass spectrometry results for unidentified organic compounds in sample AE09093 on May 10, 2002.

NYC-WTC_000044902–000044925

Folder label: “GCMS X 4/30/02 A 5/8/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\MSDCHEM\1\DATA\050802\9093 .D Vial: 15 Acq On 9 May 2002 2:49 am Operator: Mclean Sample 4/30 eh Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L

Peak Number 6 1,5-Naphthalenedithiole Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 22.58 0.30 ug/L 414925 Phenanthranene- dl 0 22.95 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,5-Naphthalenedithiole 192 C10H8S2 1000223-69-5 64 2 Bitoscanate 192 C8H4N2S2 004044-65-9 50 3 2,5-Dihydrophosphole, 3-methyl-1... 192 C11H13OP 1000196-97/5 45 4 Thiophene, 2-[2-(3-thienyl)ethen. .. 192 C10H8S2 116854-09-2 42 Abundance Scan 3319 (22.580 min): 9093.D (-3312) (-) m/z 192.10 100.00% 192

5000 ......... n....... I [ । । I-1 | r_r ii । । । । । j i r i cq i

42 52 66 82 96 146 160 22.20 22.40 22.60 22.80 23.00

m/z-> 0 I | I’l II | I I I I | I'l I I | I I I I | I H I | I I 1I |'I I I I [ I 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 118 I [ I I I I I I I I I I I I I I I > 1111111111111'j 'i 1111111111 I m/z 191.10 A 21.42% Abundance #80950: 1,5-Naphthalenedithiole 192

5000 1 ! 1 1 ‘ 1 I ' 159 22.20 22.40 22 60 22.80 23.00 115 128 m/ Z 193.10 15.93% 40 57 147 69 79 96 106 rH I'l l 1 I l' ■ 177 0 I | I I I < } ! ' I ! I1]1!1 I 'l I |' I I ' J I | I -------- I I I* I I I I I )' I m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80930: Bitoscanate 192 I | । । । । । ' । । । । । I I I | r-1 I i । i 22.20 22.40 22.60 22.80 23.00 5000 m/z 14 6.10 14.42% 134 90 160 26 39 50 63 75 0+ -- . 107116 rr11'| I■ । Ji । — —t ।'i "i । 1 148 I I I r I I I I I I 4T 110’211011’11 m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80965: 2,5-Dihydrophosphole, 3-methyl-1 -oxo-1 -phenyl- I[IlkldI I I I III IIII I 192 22.20 22.40 22.60 22.80 23.00 164 m/z 96.00 11.93% 5000 99 115 47 77 177 67 125 134 146

m/z-> 27 0 TIWTTTTTTr 38. nr l. +87 155, ’l I I I I I I I I I I I I ' I ' 1 1 1 I ' 1 1 ' I ' 1 ' 1 I ' 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 22.20 22.40 22.60 22.80 23.00

9093.D 050102.M Thu May 09 13:33:27 2002 Page 9

NYC-WTC_000044915

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NYC-WTC_000044915Source: NYC Law Department, mirrored locally

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