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GCMS analysis results for sample AE11278, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE11278 conducted on May 22, 2002, including surrogate recovery data.

NYC-WTC_000024692–000024705

Folder label: “GCMS X 5/13/02 A 5/15/02

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Scanned page image, NYC-WTC_000024703
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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11278.D Vial: 12 Acq On : 15 May 2002 10:41 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 6 Anthracene-dlO- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 31.95 0.31 ug/1 32699 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene-dlO- 188 C14D10 001719-06-8 58 2 Phehanthrene-dlO 188 C14D10 001517-22-2 52 3 Antipyrine 188 C11H12N2O 000060-80-0 27 4 Antipyrine 188 C11H12N2O 000060-80-0 25 Abundance Scan 4914 (31.952 min): 11278. D (-4908) (-) m/z 188.10 100.00% 188

5000 80 94 160 ■ i । • i > ■ > > i > 54 66 31.60 31.80 32.00 32.20

m/z-> U'",,,. ........... .. --- ‘1‘ ‘/1‘111111‘‘1‘4 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ■p-TT m/z 160.10 24.26% Abundance #79826: Anthracene-d10- 188

5000 +31.60 31.80 32.00 32.20 m/z 80.00 23.45% 80 94 160 66 11" " 111" 11'' 146.44 170179.— --H 1' I' "108118 17 30 42 52 132 ' I" " 111" I'"1111111111 mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #79827: Phenanthrene-d10 188

31.60 31.80 32.00 32.20 5000 m/Z 94.10 22.65%

80 94 160 30 42 52 66 11 108118 132 146 1 170179/1 mmTTTTTTTTHH '1" 11 ■ ■11" ■' r ■" 11"11111' 11 r’l’TT’ ।' 1111111 uh n/z-> Abundance 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 #79725: Antipyrine 188 A “i 1 ■ ■ > r'* * < । ■ 31.60 31.80 32.00 32.20 96 m/ z 189.00 21.32% 5000 77 56 105 27 39 67 m/z—> ............. a TThmPmmmm Ol 130 145 159 173 ,। i I, 115 IL 10 20 30 40 50 60 70 80 90 100110 120 130 140 150 160 170 180 190 '11' " ’ - 31,60 31.80 32.00 32.20

11278.D SCAN020507.M Thu May 16 09:56:22 2002 Page 8

NYC-WTC_000024703

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NYC-WTC_000024703Source: NYC Law Department, mirrored locally

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