GCMS analysis results for sample AE11278, May 2002

NYC 9/11 Public Portal Document Library searen Compound Report

Data File : C:\MSDCHEM\l\DATA\020515\11278.D Vial: 12 Acq On : 15 May 2002 10:41 pm Operator: Nefliu Sample : sample Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 7 dl-2-Ethylhexyl chloroformate Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

42.53 1.94 ug/1 126164 Perylene-dl2 43.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 dl-2-Ethylhexyl chloroformate 192 C9H17C1O2 024468-13-1 27 2 3-Octen-2-one, 4-(methylamino)- 155 C9H17NO 024985-58-8 22 3 1,2 ,4-Triazolo[4,3-a]pyridine-3(... 185 C6H4C1N3S 022841-91-4 22 4 3-Piperidinone, 1-acetyl-6-methyl - 155 C8H13NO2 054751-97-2 14 Abundance Scan 6715 (42.534 min): 11278.D (-6708) (-) m/z 185.20 100.00% 57 185 70

5000 43 ......... 84 112 98 [ 125 143 297 42.20 42.40 42.60 42.80 1 I ' 11'fr l"l 11 4-4-H—+r 1‘II* k 1, .11 .■. I ‘ ‘‘I 207 232 i ■ ■ r ■ i ■ ■' ■ i I 1 ° 1 1 1 1 1 '' 1 1 m/z 57.10 89.48% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #17577: dl-2-Ethylhexyl chloroformate 57 70 112

5000 83 43 42.20 42.40 42.60 42.80 m/z 70.10 66.92% 97 129 149 192............................... • i • • ■ ■ I rem i rJ TTI**II*I|u m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #24693: 3-Octen-2-one, 4-(methylamino)- _ ... । 71 113 43 98 126 140 42.20 42.40 42.60 42.80 5000 56 155 m/z55.10 59.61% 84

— 1131 nz-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #79124:1,2,4-Triazolo[4,3-a]pyricline-3(2H)-thione, 8-chloro- 185 k AarW 4hk*r mp AAMi , MMWhrylh 42.20 42.40 42.60 42.80 m/ z 71.20 58.09% 5000 127 64 92 112 + 44.78.1441141 _uuttt . / -huhnquu k 26 39 158 ml)......1 ‘I' " I " " I I ' ' ' ■ I 1 1 1 1 I ‘1 1 1 11 /z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 42.20 42.40 42.60 42.80

11278.D SCAN020507.M Thu May 16 09:56:22 2002 Page 9

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