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GCMS results for sample AE11482, May 29, 2002

Machine-extracted title · confidence 100%

Laboratory report of GCMS analysis for sample AE11482 conducted on May 29, 2002.

NYC-WTC_000022588–000022597

Folder label: “GCMS X 5/17/12 A 5/21/02

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NYC 9/11 Public Portal Document ulprary searen Compound Report

Data File : C:\MSDCHEM\l\DATA\020521\11482.D vial: 16 Acq On : 21 May 2002 11:11 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 Anthracene, 2-methyl- Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 31.10 0.29 ug/1 29079 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Anthracene, 2-methyl- 192 C15H12 000613-12-7 53 2 2-Propenal, 3-(3,4-dimethoxyphen. . . 192 C11H1203 004497-40-9 52 3 Pyrazine, tetraethyl- 192 C12H20N2 038325-19-8 42 4 5H-Dibenzo [a, d] cycloheptene 192 C15H12 000256-81-5 40 Abundance Scan 4769(31.100 min): 11482.D (-4757) (-) m/z 192.10 100.00% 19/2 VJ /

5000 146 1 1 i ■ ■ -r-r-p-r 38 66 76 86 94 120

miz-> 0 ******mHmm 160

20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 . 4 30.80 31.00 31.20 31.40 m/Z 191.00 24.53% Abundance #125845: Anthracene, 2-methyl- 192

5000 1 1 I ■ ■ ’I * ' 30.80 31,00 31.20 31.40 1 m/z 146.10 22.46%

niz-> 66 75 8/7 115 126 139 152 155 176 0 ■ I' ’11111'k I •''11" '' I'TTTHTTTTTTTTHTTTTTTHTTHTT 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 . U Abundance #80953:2-Propenal, 3-(3,4-dimethoxyphenyl)- 192 ................. .... ................... 161 30.80 31.00 31.20 31.40 5000 m/z 193.30 16.53% 77 91 121 149 177 52 64 138

n/z-> 0 l — I ‘ ‘1 ‘ 1 * HHHllmr ■" i ■' ■' i 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 Abundance #80990: Pyrazine, tetraethyl- 192 30.80 31.00 31,20 31.40 177 m/z 66.00 9.92% 5000 41 67 29 53 .. 81 93 107 121 133 149 163 /z-> 0 Tttmr — 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 1 30.80 31.00 31.20 31.40

11482.D SCAN020521.M Fri May 24 09:38:47 2002 Page 4

NYC-WTC_000022595

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NYC-WTC_000022595Source: NYC Law Department, mirrored locally

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