GCMS scan comments for sample AE11480, May 29, 2002

NYC 9/11 Public Portal Document ulprary search Compound Report Data File : C:\MSDCHEM\1\DATA\020521\11480.D Vial: 14 Acq On : 21 May 2002 9:12 pm Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020521.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 7 Phenanthrene-diO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 31.96 0.36 ug/1 36159 Phenanthrene-dl0 31.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1Phenanthrene-dI0 188 C14D10 001517-22-2 64 2 Anthracene-diO- 188 C14D10 001719-06-8 59 3 Selenide, ethyl 1-methyl-1-pente... 188 C8H12Se 025128-48-7 53 4 Benzene, 1 -bromo-4-methoxy- ____________ 186 C7H7BrO 000104-92-7 43 Abundance Scan 4915 (31.957 min): 11480.D (-4907) (-) m/z 188.20 100.00% 188

5000

94 136158 31.60 31.80 32.00 32.20

m/z-> 0- 4050 SL 100 — 207 150 200 I ‘ 250 299 300 350 400 422 m/ z 184.00 20.84% Abundance #79827: Phenanthrene-d10 188

5000 ' | T . , r J i . . J j <-1 -I I J . r i , [ I 31.60 31.80 32.00 32.20 80 160 18.63% o1 3052,,100 1321 , . —t—r | 14 । Tpl |- -i—[—i' ‘ । T i—P miz-> 50 100 150 200 250 . 300 350 400 Abundance #79826: Anthracene-d10- 108 ‘1 i ■ ' 1 1 i 1 ' 1 ' i ' 31.60 31.80 32.00 32.20 5000 m/z 189.10 13.74%

94 160 . 17 4266, 1 ,,132,4, J 0- 1 ' 1 ' I ' ’ ′ 1 r ' 1 1 IT n/z-> 50 100 150 200 250 300 350 400 ........................ ........................ Abundance #79821: Selenide, ethyl 1-methyl-1-penten-3-ynyl 188 31.60 31.80 32.00 32.20 m/z 92.20 13.37% 5000

79 159

0 Li I ■ 127,1311 4 l,., m/z-> 50 100 150 200 250 300 350 400 31,60 31.80 32.00 32.20

11480.D SCAN020521.M Fri May 24 09:32:18 2002 Page 9

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