GCMS analysis results for sample AE11155, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\020515\11155.D Vial: 21 Acq On : 16 May 2002 7:34 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 2 1-Propanesulfonic acid, met.. Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 4.30 3.49 ug/1 261982 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Propan ulfonic acid, methyl e... 138 C4H10O3S 002697-50-9 4 2 Propane,. l-chloro-2-methyl - 92 C4H9C1 000513-36-0 4 3 Hydrogen azide 43 HN3 007782-79-8 4 4 3,5-Nonadien-7-yn-2-0l, (E,E)- 136 C9H120 043142-43-4 3 Abundance Scan 208 (4.301 min): 11155.D (-204) (-) m/z 43.10 100.00% 43

5000

1 ■ 1 i 1 ■ ■ 1 i 1 1 1 1 i 1 ' 1 1 i 1 1 1 1 i

79 95 138 4.00 4.20 4.40 4.60 36. 55 63 104 123 ' 1 i 1 ' ' ' i ' ' ' ■ i ' ' ' 'I '■i■ ‘ '1 i ■ 1 • ■ i ■ r ' ' i1 ■ ' ' i 4 ■i' r '1i■■ ■ 1 i ,i 1 1 i । । I ! । । । । m/z 42.10 17.02% iz-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140

U Abundance #4067:1-Propanesulfonic acid, methyl ester 43

5000 00PTF *PA —TTPM 27 4.00 4.20 4.40 4.60 15 97 m/ z 95.00 7.52%

. 1 -11,. 50 59 RR 79 iz-> ' 1 1 1 1 10 20 30 40 50 .. X60'S70... 80I.....90 .100 107110 120 130 138140 '' ''i1 ■ I ।। । ।i ।,

Abundance #109246: Propane, 1-chloro-2-methyl- 43 IITTIII1I 1 1 I ' TT 4.00 4.20 4.40 4.60 5000 m/z 93.00 6.63% 27

1 1 I " " I 1 1 1 130140 .56 63 77 91 1 ‘ ' T' ' 1 1 ’ i ’ ’’ ti I i | | i . i | . i . I । i i n-pi i i । i . n/z-> 10 20 50 60 70 80 90 100 110 120 130 140 Abundance #3862: Hydrogen azide T—1 43 4.00 4.20 4.40 4.60 m/z 137.90 5.62% 5000 15 28

n/z-> TT-p- 10 ■ i' ■ 20 130 40 1 '' i' ' ' ‘ i '''' i ' ' ' 1 I 1 1 ' ' 1 1 1 1 ' 111 1 1 I ' ' 1 1 1 1 ' ' 1 1 1 ‘' 1 11 1 50 60 70 80 90 100 110 120 130 140 4.00 4.20 4.40 4.60

11155.D SCAN020507.M Thu May 16 09:34:56 2002 Page 4

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