GCMS analysis results for sample AE11155, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C : \MSDCHEM\1\DATA\020515 11155 .D Vial: 21 Acq On : 16 May 2002 7:34 am Operator: Nefliu Sample .- sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e

Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1 ********************************************************************* Peak Number 1 Acetonitrile, dichloro- Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

3.64 0.56 ug/1 42339 1,4-Dichlorobenzene-d4 11.38

Hit# of 5 Tentative ID MW MolForm CAS# Qual • 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 45 2 Acetnitrile, dichloro- 109 C2HC12N 003018-12-0 9 3 All mercaptan 74 C3H6S 000870-23-5 5 4 Th/irane, methyl- 74 C3H6S 001072-43-1 3 Abundane Scan 96 (3.643 min): 11155.D (-93) (-) m/z 74.00 100.00% 74

5000 47

s MMpe r, । । , Hl 320 501 3.20 3.40 3.60 3.80 4.00 i ■ 1 ' 1 m/z 47.05 45.94% mlz-> 0 50 100 150 200 250 300 350 400 450 500 Abundance #28338: Acetonitrile, dichloro- 74 MMopto 5000 i ■ ' ■ ■ i ' '

47 3.20 3.40 3.60 3.80 4.00 m/ z 82.00 45.49% 108 nz-> 0 50 100 150 200 250 300 . 350 400 450 500 Abundance #115342: Acetonitrile, dichloro- 74 » f , 44/, . . , ,, , p h 35 3.20 3.40 3.60 3.80 4.00 5000 m/z 76.00 40.22%

niz-s 0 50 100 150 200 250 300 350 400 450 500 Abundance #28161: Allyl mercaptan y 4. 41 74 3.20 3.40 3.60 3.80 4.00 m/z 84.00 36.09%

5000 LMMonop..,. A j i 1 1 ■ 1 m/z—> 0 50 100 150 200 250 300 350 400 450 500 3.20 3.40 3.60 3.80 4.00

11155.D SCAN020507.M Thu May 16 09:34:55 2002 Page 3

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