GCMS quantitation results for sample AE10301, May 2002

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Data File : C:\MSDCHEM\1\DATA\020516\10301.D Vial: 24 Acq On : 17 May 2002 8:04 am Operator: Nefliu Sample : sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: rteint.e Quant Method : C:\MSDCHEM\1\METHODS\SCAN020507.M (RTE Integrator) Title : Method 508 GC/MS Scan Library : C:\DATABASE\nist98.1

Peak Number 1 Acetonitrile, dichloro- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

3.64 0.28 ug/1 14460 1,4-Dichlorobenzene-d4 11.38 Hit# of 5 Tentative ID MW MolForm CAS# Qual

" 1 Acetonitrile, dichloro- 109 C2HC12N 003018-12-0 38 2 Allyl mercaptan 74 C3H6S 000870-23-5 7 3 Thiirane, methyl- 74 C3H6S 001072-43-1 4 4 Ethanethiol, 2-amino-, hydrochlo... 113 C2H8C1NS 000156-57-0 4 Abundance Scan 96 (3.643 min): 10301.D (-92) (-) m/ z 74.00 100.00% ' 74 82 5000 47 35 41 ——— 58 . .......... 3.20 MAA......... 3.40 3.60 3.80 4.00

n/z->10 20 30I 40 50 — 60 70 -H 90 80 100 110 m/z 82.00 55.78% Abundance #28338: Acetonitrile, dichloro- 74

5000 82 A A 47 3.20 3.40 3.60 3.80 4.00 m/ z 47.00 39.61% 35 12 .26.,30 I,140... 150....6062....70 ' TIB AMMnWjlu , 108 1 1 I 1 1 1 1 I 1 1 ■ । 1 1 ■ ■ ।11 11' i 11111 mlz-> 10 20I 80 90 100 110 Abundance #28161: Allyl mercaptan 41 74 i ■ ■ 1 1 i ' ■ 3.20 3.40 3.60 3.80 4.00 5000 m/ z 35.10 32.98%

47 27 33 । ---441+1153.58,48941 1‘ < i ■ ■ ■ ■ i • ■ ■ ■ I r । । । । । । । । m/z-> 10 20 30 40I 50 60 70 80 90 100 110 Abundance #115343: Thiirane, methyl- 41 74 320 3.40 3.60 3.80 4.00 m/z 76.00 23.19% 5000

47 27 2 , m/z—> -33lll 10 20 30 40 1153.58.68 50 60 70 1 80 90 100 110 3.20 3.40 3.60 3.80 4.00

10301.D SCAN020507.M Fri May 17 10:51:24 2002 Page 3

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